dicyclopropylmethyl N-(tert-butoxycarbonyl)-O-[(methylsulfanyl)methyl]-D-tyrosinate

Base Information

Chemical Name:dicyclopropylmethyl N-(tert-butoxycarbonyl)-O-[(methylsulfanyl)methyl]-D-tyrosinate
CAS No.:1417188-54-5
Molecular Formula:C₂₃H₃₃NO₅S
Molecular Weight:435.585
Hs Code.:

Synonyms:dicyclopropylmethyl N-(tert-butoxycarbonyl)-O-[(methylsulfanyl)methyl]-D-tyrosinate

Suppliers and Price of dicyclopropylmethyl N-(tert-butoxycarbonyl)-O-[(methylsulfanyl)methyl]-D-tyrosinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dicyclopropylmethyl N-(tert-butoxycarbonyl)-O-[(methylsulfanyl)methyl]-D-tyrosinate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dicyclopropylmethyl N-(tert-butoxycarbonyl)-O-[(methylsulfanyl)methyl]-D-tyrosinate

There total 3 articles about dicyclopropylmethyl N-(tert-butoxycarbonyl)-O-[(methylsulfanyl)methyl]-D-tyrosinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1241677-97-3
N,O-bis(tert-butoxycarbonyl)-D-tyrosine

: 1417188-54-5
dicyclopropylmethyl N-(tert-butoxycarbonyl)-O-[(methylsulfanyl)methyl]-D-tyrosinate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

2: piperidine / dichloromethane / 3 h / 20 °C

3: sodium iodide; potassium tert-butylate / N,N-dimethyl-formamide; tetrahydrofuran / 2 h / 0 - 20 °C

With piperidine; dmap; potassium tert-butylate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1417188-42-1
dicyclopropylmethyl N,O-bis(tert-butoxycarbonyl)-D-tyrosinate

: 1417188-54-5
dicyclopropylmethyl N-(tert-butoxycarbonyl)-O-[(methylsulfanyl)methyl]-D-tyrosinate

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / dichloromethane / 3 h / 20 °C

2: sodium iodide; potassium tert-butylate / N,N-dimethyl-formamide; tetrahydrofuran / 2 h / 0 - 20 °C

With piperidine; potassium tert-butylate; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1417188-54-5
dicyclopropylmethyl N-(tert-butoxycarbonyl)-O-[(methylsulfanyl)methyl]-D-tyrosinate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / water; isopropyl alcohol / 37 °C / pH 11.5 - 12

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

3: piperidine / dichloromethane / 3 h / 20 °C

4: sodium iodide; potassium tert-butylate / N,N-dimethyl-formamide; tetrahydrofuran / 2 h / 0 - 20 °C

With piperidine; dmap; potassium tert-butylate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium iodide; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;