N-[(1-benzyl-1H-tetrazol-5-yl){4-[2-(3-methyl-3H-diaziren-3-yl)ethoxy]phenyl}methyl]-N-(2-propyn-1-yl)acetamide

Base Information

Chemical Name:N-[(1-benzyl-1H-tetrazol-5-yl){4-[2-(3-methyl-3H-diaziren-3-yl)ethoxy]phenyl}methyl]-N-(2-propyn-1-yl)acetamide
CAS No.:1620482-58-7
Molecular Formula:C₂₄H₂₅N₇O₂
Molecular Weight:443.508
Hs Code.:

Synonyms:N-[(1-benzyl-1H-tetrazol-5-yl){4-[2-(3-methyl-3H-diaziren-3-yl)ethoxy]phenyl}methyl]-N-(2-propyn-1-yl)acetamide

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Chemical Property of N-[(1-benzyl-1H-tetrazol-5-yl){4-[2-(3-methyl-3H-diaziren-3-yl)ethoxy]phenyl}methyl]-N-(2-propyn-1-yl)acetamide

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Technology Process of N-[(1-benzyl-1H-tetrazol-5-yl){4-[2-(3-methyl-3H-diaziren-3-yl)ethoxy]phenyl}methyl]-N-(2-propyn-1-yl)acetamide

There total 3 articles about N-[(1-benzyl-1H-tetrazol-5-yl){4-[2-(3-methyl-3H-diaziren-3-yl)ethoxy]phenyl}methyl]-N-(2-propyn-1-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1620482-54-3
N-[(1-benzyl-1H-tetrazol-5-yl){4-[2-(3-methyl-3H-diaziren-3-yl)ethoxy]phenyl}methyl]-2-propyn-1-amine

: 75-36-5
acetyl chloride

: 1620482-58-7
N-[(1-benzyl-1H-tetrazol-5-yl){4-[2-(3-methyl-3H-diaziren-3-yl)ethoxy]phenyl}methyl]-N-(2-propyn-1-yl)acetamide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja505517t

Reference yield:

: 1620483-11-5
{4-[2-(3-methyl-3H-diaziren-3-yl)ethoxy]phenyl}methanol

: 1620482-58-7
N-[(1-benzyl-1H-tetrazol-5-yl){4-[2-(3-methyl-3H-diaziren-3-yl)ethoxy]phenyl}methyl]-N-(2-propyn-1-yl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfur trioxide pyridine complex; triethylamine / ethyl acetate; dimethyl sulfoxide / 0.33 h / 0 - 20 °C / Inert atmosphere

2: trimethylsilylazide / methanol / 0 - 20 °C / Inert atmosphere

3: pyridine / dichloromethane / 20 °C / Inert atmosphere

With pyridine; trimethylsilylazide; sulfur trioxide pyridine complex; triethylamine; In methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/ja505517t

Reference yield:

: 1620483-12-6
4-[2-(3-methyl-3H-diaziren-3-yl)ethoxy]benzaldehyde

: 1620482-58-7
N-[(1-benzyl-1H-tetrazol-5-yl){4-[2-(3-methyl-3H-diaziren-3-yl)ethoxy]phenyl}methyl]-N-(2-propyn-1-yl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilylazide / methanol / 0 - 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 20 °C / Inert atmosphere

With pyridine; trimethylsilylazide; In methanol; dichloromethane;
DOI:10.1021/ja505517t