C₂₁H₃₆O₈

Base Information

Chemical Name:C₂₁H₃₆O₈
CAS No.:1313484-37-5
Molecular Formula:C₂₁H₃₆O₈
Molecular Weight:416.512
Hs Code.:

C<sub>21</sub>H<sub>36</sub>O<sub>8</sub>

Synonyms:C₂₁H₃₆O₈

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Chemical Property of C₂₁H₃₆O₈

Chemical Property:

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Technology Process of C₂₁H₃₆O₈

There total 23 articles about C₂₁H₃₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1313484-36-4
C₁₄H₂₆O₇

: 98-89-5
Cyclohexanecarboxylic acid

: 1313484-37-5
C₂₁H₃₆O₈

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 19h; Inert atmosphere;
DOI:10.1039/c1cc11388g

Reference yield: 86.0%

: C₁₅H₂₄O₅

: 107-30-2
chloromethyl methyl ether

: 1313484-37-5
C₂₁H₃₆O₈

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 15h; Reflux; Inert atmosphere;
DOI:10.3762/bjoc.10.15

Reference yield:

: 928618-22-8
(2'S,3'S,4R,5R)-2-hydroxymethyl-4-O,5-O-(2',3'-dimethoxybutane-2',3'-diyl)-4,5-dihydroxycyclohex-2-en-1-one

: 1313484-37-5
C₂₁H₃₆O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: dmap; triethylamine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere

2.1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 - 0 °C / Inert atmosphere

3.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.25 h / 0 °C / Inert atmosphere

4.1: triphenylphosphine; diethylazodicarboxylate; 4-nitro-benzoic acid / toluene / 15 h / 20 °C / Inert atmosphere

4.2: 2 h / 20 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane; water / 0.17 h / 20 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine; sodium iodide / tetrahydrofuran / 4.5 h / 20 °C / Reflux; Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

8.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 19 h / 20 °C / Inert atmosphere

With dmap; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium tetrahydroborate; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; sodium iodide; lithium hexamethyldisilazane; diethylazodicarboxylate; 4-nitro-benzoic acid; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 3.1: Luche reduction / 4.2: Mitsunobu reaction;
DOI:10.1039/c1cc11388g