3-O-[6-O-(2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl]-sn-glycerol

Base Information

Chemical Name:3-O-[6-O-(2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl]-sn-glycerol
CAS No.:544687-00-5
Molecular Formula:C₇₃H₈₂O₁₃Si
Molecular Weight:1195.53
Hs Code.:

Synonyms:3-O-[6-O-(2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl]-sn-glycerol

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Chemical Property of 3-O-[6-O-(2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl]-sn-glycerol

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Technology Process of 3-O-[6-O-(2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl]-sn-glycerol

There total 3 articles about 3-O-[6-O-(2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl]-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1,2-O-isopropylidene-3-O-[6-O-(2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl]-sn-glycerol

: 544687-00-5
3-O-[6-O-(2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl]-sn-glycerol

Guidance literature:: With acetic acid; at 80 ℃; for 1.5h;
DOI:10.1002/anie.200390243

Reference yield: 77.0%

: 1552275-51-0
C₇₉H₉₀O₁₃Si

: 544687-00-5
3-O-[6-O-(2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl]-sn-glycerol

Guidance literature:: With acetic acid; In water; toluene; at 90 ℃; for 3h;
DOI:10.3390/molecules181113546

Reference yield:

: 100-39-0
benzyl bromide

: 544687-00-5
3-O-[6-O-(2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl]-sn-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / NaH / dimethylformamide

2: 78 percent / aq. AcOH / 1.5 h / 80 °C

With sodium hydride; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1002/anie.200390243