(ethoxycarbonyloxy)methyl (4S,5S)-5-[(S)-2-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-3-methylbutyl]-4-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}oxazolidine-3-carboxylate

Base Information

Chemical Name:(ethoxycarbonyloxy)methyl (4S,5S)-5-[(S)-2-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-3-methylbutyl]-4-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}oxazolidine-3-carboxylate
CAS No.:1301763-88-1
Molecular Formula:C₃₆H₅₉N₃O₁₁
Molecular Weight:709.878
Hs Code.:

(ethoxycarbonyloxy)methyl (4S,5S)-5-[(S)-2-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-3-methylbutyl]-4-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}oxazolidine-3-carboxylate

Synonyms:(ethoxycarbonyloxy)methyl (4S,5S)-5-[(S)-2-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-3-methylbutyl]-4-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}oxazolidine-3-carboxylate

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Chemical Property of (ethoxycarbonyloxy)methyl (4S,5S)-5-[(S)-2-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-3-methylbutyl]-4-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}oxazolidine-3-carboxylate

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Technology Process of (ethoxycarbonyloxy)methyl (4S,5S)-5-[(S)-2-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-3-methylbutyl]-4-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}oxazolidine-3-carboxylate

There total 2 articles about (ethoxycarbonyloxy)methyl (4S,5S)-5-[(S)-2-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-3-methylbutyl]-4-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}oxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 1301763-73-4
(4S,5S)-5-((2S)-2-{[(3-amino-2,2-dimethyl-3-oxopropyl)amino]carbonyl}-3-methylbutyl)-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidine

: 82619-14-5
ethoxycarbonyloxymethyl iodide

: 1301763-88-1
(ethoxycarbonyloxy)methyl (4S,5S)-5-[(S)-2-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-3-methylbutyl]-4-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}oxazolidine-3-carboxylate

Guidance literature:: carbon dioxide; (4S,5S)-5-((2S)-2-{[(3-amino-2,2-dimethyl-3-oxopropyl)amino]carbonyl}-3-methylbutyl)-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidine; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.833333h;

ethoxycarbonyloxymethyl iodide; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 173334-57-1
(2S,4S,5S,7S)-5-Amino-4-hydroxy-2-isopropyl-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-nonanoic acid (2-carbamoyl-2-methyl-propyl)-amide

: 1301763-88-1
(ethoxycarbonyloxy)methyl (4S,5S)-5-[(S)-2-(3-amino-2,2-dimethyl-3-oxopropylcarbamoyl)-3-methylbutyl]-4-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}oxazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; tetrahydrofuran / 5 h / Cooling with ice

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.83 h / 20 °C

2.2: 20 °C

With caesium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide;