(13aS)-5,8,13,13aα-Tetrahydro-2,11-dimethoxy-6H-dibenzo[a,g]quinolizine-1,10-diol

Base Information

• Chemical Name: (13aS)-5,8,13,13aα-Tetrahydro-2,11-dimethoxy-6H-dibenzo[a,g]quinolizine-1,10-diol
• CAS No.: 27498-04-0
• Molecular Formula: C₁₉H₂₁NO₄
• Molecular Weight: 327.38
• Mol file: 27498-04-0.mol

Synonyms:6H-Dibenzo[a,g]quinolizine-1,11-diol,5,8,13,13a-tetrahydro-2,10-dimethoxy-, (S)-; Caseamine (8CI); (-)-Caseamine

Chemical Property of (13aS)-5,8,13,13aα-Tetrahydro-2,11-dimethoxy-6H-dibenzo[a,g]quinolizine-1,10-diol

Chemical Property:

• PSA: 62.16000
• LogP: 2.70840

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (13aS)-5,8,13,13aα-Tetrahydro-2,11-dimethoxy-6H-dibenzo[a,g]quinolizine-1,10-diol

There total 1 articles about (13aS)-5,8,13,13aα-Tetrahydro-2,11-dimethoxy-6H-dibenzo[a,g]quinolizine-1,10-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + nor-(S)-(+)-crassifoline → (S)-(?)-clarkeanidine (99615-99-3) + (-)-caseamine (27498-04-0)

Guidance literature:

In 2,2,2-trifluoroethanol; at 20 ℃; for 5h;

DOI:10.1021/acs.joc.8b02378

Reference yield: 20.3%

diazomethane (186581-53-3,908094-01-9,334-88-3) + (-)-caseamine (27498-04-0) → (-)-caseadine (34413-12-2) + (-)-O-methyl caseadine (19637-57-1)

Guidance literature:

In methanol; diethyl ether;

DOI:10.1016/0031-9422(88)80486-2

upstream raw materials:

formaldehyd

Downstream raw materials:

(-)-caseadine

(-)-O-methyl caseadine

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