6-nitro-1,2,3-benzotriazin-4(1H)-one

Base Information

Chemical Name:6-nitro-1,2,3-benzotriazin-4(1H)-one
CAS No.:91532-29-5
Molecular Formula:C7H4N4O3
Molecular Weight:192.134
Hs Code.:

Synonyms:

Suppliers and Price of 6-nitro-1,2,3-benzotriazin-4(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 6 raw suppliers

Chemical Property of 6-nitro-1,2,3-benzotriazin-4(1H)-one

Chemical Property:

Vapor Pressure:3.28E-06mmHg at 25°C
Boiling Point:387.5°Cat760mmHg
Flash Point:188.1°C
Density:1.82g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-nitro-1,2,3-benzotriazin-4(1H)-one

There total 5 articles about 6-nitro-1,2,3-benzotriazin-4(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 41339-17-7
5-nitro-1H-indazol-3-amine

: 91532-29-5
6-nitrobenzo[d][1,2,3]triazin-4(3H)-one

Guidance literature:: With N-bromophthalimide; ammonium cerium (IV) nitrate; In water; acetonitrile; at 20 ℃; for 16h; Sealed tube;
DOI:10.1021/acs.orglett.8b02813

Reference yield: 56.0%

: 16313-65-8
2-amino-5-nitrobenzamide

: 91532-29-5
6-nitrobenzo[d][1,2,3]triazin-4(3H)-one

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 0 - 65 ℃; for 8h;
DOI:10.1039/d1ob00968k

Reference yield:

: 616-79-5
2-amino-5-nitro-benzoic acid

: 91532-29-5
6-nitrobenzo[d][1,2,3]triazin-4(3H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 19 h / -10 - 20 °C

2.1: ammonium carbonate / 1,4-dioxane / 60 °C

3.1: sodium nitrite; hydrogenchloride / water; N,N-dimethyl-formamide / 1.67 h / 0 °C

3.2: 0.25 h / pH 10

With hydrogenchloride; ammonium carbonate; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/acs.jafc.5b01762