Technology Process of C24H21N5O6
There total 5 articles about C24H21N5O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(l) iodide; N-ethyl-N,N-diisopropylamine;
In
acetonitrile;
at 20 ℃;
for 16h;
Inert atmosphere;
DOI:10.1039/c2ob27155a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: oxalyl dichloride / dichloromethane / 5 h / 20 °C / Inert atmosphere
2: triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
3: sodium azide; copper(l) iodide; sodium L-ascorbate; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 16 h / 20 °C / Inert atmosphere
4: copper(l) iodide; N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 20 °C / Inert atmosphere
With
copper(l) iodide; sodium azide; oxalyl dichloride; sodium L-ascorbate; triethylamine; N-ethyl-N,N-diisopropylamine; N,N`-dimethylethylenediamine;
In
dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c2ob27155a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide; copper(l) iodide; sodium L-ascorbate; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 16 h / 20 °C / Inert atmosphere
2: copper(l) iodide; N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 20 °C / Inert atmosphere
With
copper(l) iodide; sodium azide; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; N,N`-dimethylethylenediamine;
In
water; dimethyl sulfoxide; acetonitrile;
DOI:10.1039/c2ob27155a