N-benzyloxycarbonyl-1-(p-nitrobenzyl)-δ-(L-α-aminoadipyl)-S-benzyl-L-cysteine

Base Information

Chemical Name:N-benzyloxycarbonyl-1-(p-nitrobenzyl)-δ-(L-α-aminoadipyl)-S-benzyl-L-cysteine
CAS No.:87141-26-2
Molecular Formula:C₃₁H₃₃N₃O₉S
Molecular Weight:623.684
Hs Code.:

Synonyms:N-benzyloxycarbonyl-1-(p-nitrobenzyl)-δ-(L-α-aminoadipyl)-S-benzyl-L-cysteine

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Chemical Property of N-benzyloxycarbonyl-1-(p-nitrobenzyl)-δ-(L-α-aminoadipyl)-S-benzyl-L-cysteine

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Technology Process of N-benzyloxycarbonyl-1-(p-nitrobenzyl)-δ-(L-α-aminoadipyl)-S-benzyl-L-cysteine

There total 5 articles about N-benzyloxycarbonyl-1-(p-nitrobenzyl)-δ-(L-α-aminoadipyl)-S-benzyl-L-cysteine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 87141-25-1
N-benzyloxycarbonyl-1-(p-nitrobenzyl)-δ-(L-α-aminoadipyl)-S-benzyl-L-cysteine, benzhydryl ester

: 87141-26-2
N-benzyloxycarbonyl-1-(p-nitrobenzyl)-δ-(L-α-aminoadipyl)-S-benzyl-L-cysteine

Guidance literature:: With hydrogenchloride; In nitromethane; for 5h; Ambient temperature;
DOI:10.1039/P19830000941

Reference yield:

: 24325-14-2
(2S)-2-[(phenylmethoxy)carbonyl]aminoadipic acid

: 87141-26-2
N-benzyloxycarbonyl-1-(p-nitrobenzyl)-δ-(L-α-aminoadipyl)-S-benzyl-L-cysteine

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / Et₃N / dimethylformamide / 0 deg C -> room temperature, overnight

2: 64 percent / 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodi-imide / ethyl acetate

3: 98 percent / 0.2M HCl / nitromethane / 5 h / Ambient temperature

With hydrogenchloride; 1-hydroxybenzotriazol-hydrate; triethylamine; dicyclohexyl-carbodiimide; In nitromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/P19830000941

Reference yield:

: 87141-24-0
S-benzyl-L-cysteine, benzhydryl ester

: 87141-26-2
N-benzyloxycarbonyl-1-(p-nitrobenzyl)-δ-(L-α-aminoadipyl)-S-benzyl-L-cysteine

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodi-imide / ethyl acetate

2: 98 percent / 0.2M HCl / nitromethane / 5 h / Ambient temperature

With hydrogenchloride; 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide; In nitromethane; ethyl acetate;
DOI:10.1039/P19830000941