(3R,5S,6S)-3-acetoxy-5-benzyloxycarbonylamino-6-tert-butoxycarbonylaminocyclohexene

Base Information

Chemical Name:(3R,5S,6S)-3-acetoxy-5-benzyloxycarbonylamino-6-tert-butoxycarbonylaminocyclohexene
CAS No.:927395-50-4
Molecular Formula:C₂₁H₂₈N₂O₆
Molecular Weight:404.463
Hs Code.:

Synonyms:(3R,5S,6S)-3-acetoxy-5-benzyloxycarbonylamino-6-tert-butoxycarbonylaminocyclohexene

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Chemical Property of (3R,5S,6S)-3-acetoxy-5-benzyloxycarbonylamino-6-tert-butoxycarbonylaminocyclohexene

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Technology Process of (3R,5S,6S)-3-acetoxy-5-benzyloxycarbonylamino-6-tert-butoxycarbonylaminocyclohexene

There total 3 articles about (3R,5S,6S)-3-acetoxy-5-benzyloxycarbonylamino-6-tert-butoxycarbonylaminocyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7-(3,5-dinitrobenzoyl)-7-azabicyclo[4.1.0]hept-3-ene

: 927395-50-4
(3R,5S,6S)-3-acetoxy-5-benzyloxycarbonylamino-6-tert-butoxycarbonylaminocyclohexene

Guidance literature:: Multi-step reaction with 3 steps

1.1: Y(O-i-Pr)3; TMSN₃; 2,6-dimethylphenol / 6-deoxy-6-(diphenylphosphoryl)-arabino-hexitol-based ligand / various solvent(s) / 12 h / 20 °C

2.1: 4-(dimethylamino)pyridine / acetonitrile / 1 h / 20 °C

2.2: 98 percent / NaOH / acetonitrile; H₂O / 1 h / 20 °C

With dmap; 2.6-dimethylphenol; yttrium(III) isopropoxide; trimethylsilylazide; 6-deoxy-6-(diphenylphosphoryl)-arabino-hexitol-based ligand; In acetonitrile;
DOI:10.1021/ol062663c

Reference yield:

: 891831-05-3
(4S,5S)-4-azido-5-(3,5-dinitrobenzoylamino)cyclohexene

: 927395-50-4
(3R,5S,6S)-3-acetoxy-5-benzyloxycarbonylamino-6-tert-butoxycarbonylaminocyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4-(dimethylamino)pyridine / acetonitrile / 1 h / 20 °C

1.2: 98 percent / NaOH / acetonitrile; H₂O / 1 h / 20 °C

With dmap; In acetonitrile;
DOI:10.1021/ol062663c