(3R,5S,6S)-5-benzyloxycarbonylamino-6-tert-butoxycarbonylamino-3-hydroxycyclohexene

Base Information

Chemical Name:(3R,5S,6S)-5-benzyloxycarbonylamino-6-tert-butoxycarbonylamino-3-hydroxycyclohexene
CAS No.:927395-75-3
Molecular Formula:C₁₉H₂₆N₂O₅
Molecular Weight:362.426
Hs Code.:

Synonyms:(3R,5S,6S)-5-benzyloxycarbonylamino-6-tert-butoxycarbonylamino-3-hydroxycyclohexene

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Chemical Property of (3R,5S,6S)-5-benzyloxycarbonylamino-6-tert-butoxycarbonylamino-3-hydroxycyclohexene

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Technology Process of (3R,5S,6S)-5-benzyloxycarbonylamino-6-tert-butoxycarbonylamino-3-hydroxycyclohexene

There total 5 articles about (3R,5S,6S)-5-benzyloxycarbonylamino-6-tert-butoxycarbonylamino-3-hydroxycyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 927395-50-4
(3R,5S,6S)-3-acetoxy-5-benzyloxycarbonylamino-6-tert-butoxycarbonylaminocyclohexene

: 927395-75-3
(3R,5S,6S)-5-benzyloxycarbonylamino-6-tert-butoxycarbonylamino-3-hydroxycyclohexene

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 2h;
DOI:10.1021/ol062663c

Reference yield:

: 7-(3,5-dinitrobenzoyl)-7-azabicyclo[4.1.0]hept-3-ene

: 927395-75-3
(3R,5S,6S)-5-benzyloxycarbonylamino-6-tert-butoxycarbonylamino-3-hydroxycyclohexene

Guidance literature:: Multi-step reaction with 4 steps

1.1: Y(O-i-Pr)3; TMSN₃; 2,6-dimethylphenol / 6-deoxy-6-(diphenylphosphoryl)-arabino-hexitol-based ligand / various solvent(s) / 12 h / 20 °C

2.1: 4-(dimethylamino)pyridine / acetonitrile / 1 h / 20 °C

2.2: 98 percent / NaOH / acetonitrile; H₂O / 1 h / 20 °C

3.1: 99 percent / potassium carbonate / methanol / 2 h / 20 °C

With dmap; 2.6-dimethylphenol; yttrium(III) isopropoxide; trimethylsilylazide; potassium carbonate; 6-deoxy-6-(diphenylphosphoryl)-arabino-hexitol-based ligand; In methanol; acetonitrile;
DOI:10.1021/ol062663c

Reference yield:

: 891831-05-3
(4S,5S)-4-azido-5-(3,5-dinitrobenzoylamino)cyclohexene

: 927395-75-3
(3R,5S,6S)-5-benzyloxycarbonylamino-6-tert-butoxycarbonylamino-3-hydroxycyclohexene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4-(dimethylamino)pyridine / acetonitrile / 1 h / 20 °C

1.2: 98 percent / NaOH / acetonitrile; H₂O / 1 h / 20 °C

2.1: 99 percent / potassium carbonate / methanol / 2 h / 20 °C

With dmap; potassium carbonate; In methanol; acetonitrile;
DOI:10.1021/ol062663c