5-(4-(3-chloro-4-hydroxyphenylamino)quinazolin-6-yl)furan-2-carbaldehyde tosylate

Base Information

Chemical Name:5-(4-(3-chloro-4-hydroxyphenylamino)quinazolin-6-yl)furan-2-carbaldehyde tosylate
CAS No.:1440511-82-9
Molecular Formula:C₇H₈O₃S*C₁₉H₁₂ClN₃O₃
Molecular Weight:537.98
Hs Code.:

Synonyms:5-(4-(3-chloro-4-hydroxyphenylamino)quinazolin-6-yl)furan-2-carbaldehyde tosylate

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Chemical Property of 5-(4-(3-chloro-4-hydroxyphenylamino)quinazolin-6-yl)furan-2-carbaldehyde tosylate

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Technology Process of 5-(4-(3-chloro-4-hydroxyphenylamino)quinazolin-6-yl)furan-2-carbaldehyde tosylate

There total 4 articles about 5-(4-(3-chloro-4-hydroxyphenylamino)quinazolin-6-yl)furan-2-carbaldehyde tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.4%

: 1440511-81-8
5-(4-(3-chloro-4-hydroxyphenylamino)quinazolin-6-yl)furan-2-carbaldehyde

: 104-15-4
toluene-4-sulfonic acid

: 1440511-82-9
5-(4-(3-chloro-4-hydroxyphenylamino)quinazolin-6-yl)furan-2-carbaldehyde tosylate

Guidance literature:: In water; at 20 - 30 ℃;

Reference yield:

: 98556-31-1
4-chloro-6-iodoquinazoline

: 1440511-82-9
5-(4-(3-chloro-4-hydroxyphenylamino)quinazolin-6-yl)furan-2-carbaldehyde tosylate

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 1 h / Reflux

2: triethylamine; palladium 10% on activated carbon / water; 1,2-dimethoxyethane; methanol / 45 - 50 °C

3: water / 20 - 30 °C

With palladium 10% on activated carbon; triethylamine; In methanol; 1,2-dimethoxyethane; water; acetonitrile;

Reference yield:

: 3964-52-1
2-chloro 4-aminophenol

: 1440511-82-9
5-(4-(3-chloro-4-hydroxyphenylamino)quinazolin-6-yl)furan-2-carbaldehyde tosylate

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 1 h / Reflux

2: triethylamine; palladium 10% on activated carbon / water; 1,2-dimethoxyethane; methanol / 45 - 50 °C

3: water / 20 - 30 °C

With palladium 10% on activated carbon; triethylamine; In methanol; 1,2-dimethoxyethane; water; acetonitrile;