3,3-dichloro-2-phenylacryloyl chloride

Base Information

Chemical Name:3,3-dichloro-2-phenylacryloyl chloride
CAS No.:40920-45-4
Molecular Formula:C₉H₅Cl₃O
Molecular Weight:235.497
Hs Code.:

Synonyms:3,3-dichloro-2-phenylacryloyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3-dichloro-2-phenylacryloyl chloride

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Technology Process of 3,3-dichloro-2-phenylacryloyl chloride

There total 5 articles about 3,3-dichloro-2-phenylacryloyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 82549-32-4
methyl 3,3-dichloro-2-phenylacrylate

: 40920-45-4
3,3-dichloro-2-phenylacryloyl chloride

Guidance literature:: methyl 3,3-dichloro-2-phenylacrylate; With sodium hydroxide;

With thionyl chloride; Further stages.;
DOI:10.1016/j.tetlet.2008.02.014

Reference yield:

: 1603-79-8
phenylglyoxylic acid ethyl ester

: 40920-45-4
3,3-dichloro-2-phenylacryloyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: Ph₃P / 5.5 h / 60 - 65 °C

2: aq. NaOH / 1 h / Heating

With sodium hydroxide; triphenylphosphine;