(4-benzenesulfinyl-7-isopropylimino-cyclohepta-1,3,5-trienyl)isopropylamine

Base Information

• Chemical Name: (4-benzenesulfinyl-7-isopropylimino-cyclohepta-1,3,5-trienyl)isopropylamine
• CAS No.: 1229183-78-1
• Molecular Formula: C₁₉H₂₄N₂OS
• Molecular Weight: 328.478
• Mol file: 1229183-78-1.mol

Synonyms:(4-benzenesulfinyl-7-isopropylimino-cyclohepta-1,3,5-trienyl)isopropylamine

Chemical Property of (4-benzenesulfinyl-7-isopropylimino-cyclohepta-1,3,5-trienyl)isopropylamine

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4-benzenesulfinyl-7-isopropylimino-cyclohepta-1,3,5-trienyl)isopropylamine

There total 1 articles about (4-benzenesulfinyl-7-isopropylimino-cyclohepta-1,3,5-trienyl)isopropylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

isopropyl-(7-isopropylimino-4-phenylsulfanylcyclohepta-1,3,5-trienyl)amine (1036763-09-3) → (4-benzenesulfinyl-7-isopropylimino-cyclohepta-1,3,5-trienyl)isopropylamine (1229183-78-1)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃;

DOI:10.1021/om901012f

Reference yield: 98.0%

(4-benzenesulfinyl-7-isopropylimino-cyclohepta-1,3,5-trienyl)isopropylamine (1229183-78-1) + dimethyl zinc(II) (544-97-8) → 5-benzenesulfinyl-N-isopropyl-2-(isopropylamino)troponiminate zinc methyl (1229183-87-2)

Guidance literature:

In toluene; byproducts: CH4; (Ar); Schlenk technique; soln. of ligand in toluene was slowly added to soln. of Me2Zn in toluene at 0°C; slowly warmed to room temp.; stirred for 3 h; filtered; evapd.; washed (pentane); elem. anal.;

DOI:10.1021/om901012f

upstream raw materials:

isopropyl-(7-isopropylimino-4-phenylsulfanylcyclohepta-1,3,5-trienyl)amine

Downstream raw materials:

5-benzenesulfinyl-N-isopropyl-2-(isopropylamino)troponiminate zinc methyl