C₃₀H₄₉ClO₅Si

Base Information

Chemical Name:C₃₀H₄₉ClO₅Si
CAS No.:1032990-00-3
Molecular Formula:C₃₀H₄₉ClO₅Si
Molecular Weight:553.255
Hs Code.:

C<sub>30</sub>H<sub>49</sub>ClO<sub>5</sub>Si

Synonyms:C₃₀H₄₉ClO₅Si

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Chemical Property of C₃₀H₄₉ClO₅Si

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Technology Process of C₃₀H₄₉ClO₅Si

There total 9 articles about C₃₀H₄₉ClO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1032989-87-9
C₈H₁₃ClO₂

: 916323-72-3
C₂₂H₃₆O₃Si

: 1032990-00-3
C₃₀H₄₉ClO₅Si

Guidance literature:: C₈H₁₃ClO₂; With dicyclohexylboron chloride; triethylamine; In diethyl ether; at -78 - 0 ℃; for 1h; Inert atmosphere;

C₂₂H₃₆O₃Si; In diethyl ether; at -78 - -20 ℃; for 46h; Inert atmosphere;
DOI:10.1039/c2ob25100k

Reference yield:

: 5470-84-8
4-benzyloxybutanal

: 1032990-00-3
C₃₀H₄₉ClO₅Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: piperidine / 5,5-dimethyl-1,3-cyclohexadiene / 0.5 h / 160 °C / Inert atmosphere

1.2: 3.5 h / 155 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

4.1: dicyclohexylboron chloride; triethylamine / diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere

4.2: 17 h / -78 - -20 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

6.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Inert atmosphere

6.2: 5 h / 0 - 20 °C / Inert atmosphere

7.1: sodium periodate / methanol / 0.5 h / 20 °C / pH 7 / aq. buffer; Inert atmosphere

8.1: dicyclohexylboron chloride; triethylamine / diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere

8.2: 46 h / -78 - -20 °C / Inert atmosphere

With piperidine; 2,6-dimethylpyridine; sodium tetrahydroborate; sodium periodate; lithium aluminium tetrahydride; dicyclohexylboron chloride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; dichloromethane; 1.1: Knoevenagel reaction / 1.2: Knoevenagel reaction / 3.1: Dess-Martin oxidation / 4.1: Aldol condensation / 4.2: Aldol condensation / 8.1: Aldol condensation / 8.2: Aldol condensation;
DOI:10.1039/c2ob25100k

Reference yield:

: 916323-73-4
(E)-6-Benzyloxy-hex-3-enal

: 1032990-00-3
C₃₀H₄₉ClO₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: dicyclohexylboron chloride; triethylamine / diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere

1.2: 17 h / -78 - -20 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

3.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Inert atmosphere

3.2: 5 h / 0 - 20 °C / Inert atmosphere

4.1: sodium periodate / methanol / 0.5 h / 20 °C / pH 7 / aq. buffer; Inert atmosphere

5.1: dicyclohexylboron chloride; triethylamine / diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere

5.2: 46 h / -78 - -20 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium tetrahydroborate; sodium periodate; dicyclohexylboron chloride; triethylamine; In methanol; diethyl ether; dichloromethane; 1.1: Aldol condensation / 1.2: Aldol condensation / 5.1: Aldol condensation / 5.2: Aldol condensation;
DOI:10.1039/c2ob25100k