tert-butyl {6-[({[(Z)-cyano(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate

Base Information

• Chemical Name: tert-butyl {6-[({[(Z)-cyano(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate
• CAS No.: 1427201-43-1
• Molecular Formula: C₁₉H₂₀N₄O₃
• Molecular Weight: 352.393

Synonyms:tert-butyl {6-[({[(Z)-cyano(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate

Chemical Property of tert-butyl {6-[({[(Z)-cyano(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate

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Technology Process of tert-butyl {6-[({[(Z)-cyano(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate

There total 1 articles about tert-butyl {6-[({[(Z)-cyano(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

tert-butyl [6-(chloromethyl)pyridin-2-yl]carbamate + (Z)-2-(hydroxyimino)-2-phenylacetonitrile (7541-02-8) → tert-butyl {6-[({[(Z)-cyano(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate (1427201-43-1)

Guidance literature:

With caesium carbonate; potassium iodide; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃;

Reference yield: 95.0%

tert-butyl {6-[({[(Z)-cyano(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate (1427201-43-1) + N-ethylhydroxylamine trifluoroacetate → tert-butyl (6-{[({(1Z)-2-[hydroxy(ethyl)amino]-2-imino-1-(phenyl)ethylidene}amino)oxy]methyl}pyridin-2-yl)carbamate (1446190-12-0)

Guidance literature:

With potassium carbonate; In water; isopropyl alcohol; at 80 ℃; for 6h;

Reference yield: 89.0%

tert-butyl {6-[({[(Z)-cyano(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate (1427201-43-1) → (2Z)-{[(6-aminopyridin-2-yl)methoxy]imino}(phenyl)acetonitrile (1427201-44-2)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 12h; Reflux;

upstream raw materials:

(Z)-2-(hydroxyimino)-2-phenylacetonitrile

Downstream raw materials:

(2Z)-{[(6-aminopyridin-2-yl)methoxy]imino}(phenyl)acetonitrile

(1Z,2Z)-2-{[(6-aminopyridin-2-yl)methoxy]imino}-N'-hydroxy-2-phenylethanimidamide

3-[(Z)-{[(6-aminopyridin-2-yl)methoxy]imino}(phenyl)methyl]-1,2,4-oxadiazol-5(4H)-one

butyl {6-[({[(Z)-(4-methyl-5-oxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate

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