(1Z,2Z)-2-{[(6-aminopyridin-2-yl)methoxy]imino}-N'-hydroxy-2-phenylethanimidamide

Base Information

Chemical Name:(1Z,2Z)-2-{[(6-aminopyridin-2-yl)methoxy]imino}-N'-hydroxy-2-phenylethanimidamide
CAS No.:1427201-30-6
Molecular Formula:C₁₄H₁₅N₅O₂
Molecular Weight:285.305
Hs Code.:

Synonyms:(1Z,2Z)-2-{[(6-aminopyridin-2-yl)methoxy]imino}-N'-hydroxy-2-phenylethanimidamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1Z,2Z)-2-{[(6-aminopyridin-2-yl)methoxy]imino}-N'-hydroxy-2-phenylethanimidamide

Chemical Property:

Purity/Quality:

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Technology Process of (1Z,2Z)-2-{[(6-aminopyridin-2-yl)methoxy]imino}-N'-hydroxy-2-phenylethanimidamide

There total 3 articles about (1Z,2Z)-2-{[(6-aminopyridin-2-yl)methoxy]imino}-N'-hydroxy-2-phenylethanimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl [6-(chloromethyl)pyridin-2-yl]carbamate

: 1427201-30-6
(1Z,2Z)-2-{[(6-aminopyridin-2-yl)methoxy]imino}-N'-hydroxy-2-phenylethanimidamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium iodide; caesium carbonate / acetonitrile; N,N-dimethyl-formamide / 20 °C

2: trifluoroacetic acid / dichloromethane / 12 h / Reflux

3: hydroxylamine hydrochloride; potassium carbonate / isopropyl alcohol; water / 6 h / 80 °C

With hydroxylamine hydrochloride; potassium carbonate; caesium carbonate; trifluoroacetic acid; potassium iodide; In dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;

Reference yield:

: 1427201-43-1
tert-butyl {6-[({[(Z)-cyano(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate

: 1427201-30-6
(1Z,2Z)-2-{[(6-aminopyridin-2-yl)methoxy]imino}-N'-hydroxy-2-phenylethanimidamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 12 h / Reflux

2: hydroxylamine hydrochloride; potassium carbonate / isopropyl alcohol; water / 6 h / 80 °C

With hydroxylamine hydrochloride; potassium carbonate; trifluoroacetic acid; In dichloromethane; water; isopropyl alcohol;

Reference yield:

: 7541-02-8
(Z)-2-(hydroxyimino)-2-phenylacetonitrile

: 1427201-30-6
(1Z,2Z)-2-{[(6-aminopyridin-2-yl)methoxy]imino}-N'-hydroxy-2-phenylethanimidamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium iodide; caesium carbonate / acetonitrile; N,N-dimethyl-formamide / 20 °C

2: trifluoroacetic acid / dichloromethane / 12 h / Reflux

3: hydroxylamine hydrochloride; potassium carbonate / isopropyl alcohol; water / 6 h / 80 °C

With hydroxylamine hydrochloride; potassium carbonate; caesium carbonate; trifluoroacetic acid; potassium iodide; In dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;