[(dicyclohexylamino)(diisopropylamino)phosphino](trimethylsilyl)diazomethane

Base Information

Chemical Name:[(dicyclohexylamino)(diisopropylamino)phosphino](trimethylsilyl)diazomethane
CAS No.:188053-37-4
Molecular Formula:C₂₂H₄₅N₄PSi
Molecular Weight:424.685
Hs Code.:

Synonyms:[(dicyclohexylamino)(diisopropylamino)phosphino](trimethylsilyl)diazomethane

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Chemical Property of [(dicyclohexylamino)(diisopropylamino)phosphino](trimethylsilyl)diazomethane

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Technology Process of [(dicyclohexylamino)(diisopropylamino)phosphino](trimethylsilyl)diazomethane

There total 3 articles about [(dicyclohexylamino)(diisopropylamino)phosphino](trimethylsilyl)diazomethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 188053-31-8
(dicycloxeylamino)(diisopropylamino)chlorophosphine

: 18107-18-1
diazomethyl-trimethyl-silane

: 188053-37-4
[(dicyclohexylamino)(diisopropylamino)phosphino](trimethylsilyl)diazomethane

Guidance literature:: diazomethyl-trimethyl-silane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

(dicycloxeylamino)(diisopropylamino)chlorophosphine; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1021/ja9637661

Reference yield:

: 93583-22-3
(dicyclohexylamino)dichlorophosphine

: 188053-37-4
[(dicyclohexylamino)(diisopropylamino)phosphino](trimethylsilyl)diazomethane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 76 percent / tetrahydrofuran / -78 - 20 °C

2.1: BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

2.2: 82 percent / tetrahydrofuran; hexane / -78 - 20 °C

With n-butyllithium; In tetrahydrofuran; hexane; 1.1: Substitution / 2.1: Metallation / 2.2: Substitution;
DOI:10.1021/ja9637661

Reference yield:

: 4111-54-0
lithium diisopropyl amide

: 188053-37-4
[(dicyclohexylamino)(diisopropylamino)phosphino](trimethylsilyl)diazomethane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 76 percent / tetrahydrofuran / -78 - 20 °C

2.1: BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

2.2: 82 percent / tetrahydrofuran; hexane / -78 - 20 °C

With n-butyllithium; In tetrahydrofuran; hexane; 1.1: Substitution / 2.1: Metallation / 2.2: Substitution;
DOI:10.1021/ja9637661