bis(4-(imidazol-1-yl)phenyl)diazene

Base Information

• Chemical Name: bis(4-(imidazol-1-yl)phenyl)diazene
• CAS No.: 1263305-79-8
• Molecular Formula: C₁₈H₁₄N₆
• Molecular Weight: 314.349
• Mol file: 1263305-79-8.mol

Synonyms:bis(4-(imidazol-1-yl)phenyl)diazene

Chemical Property of bis(4-(imidazol-1-yl)phenyl)diazene

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of bis(4-(imidazol-1-yl)phenyl)diazene

There total 1 articles about bis(4-(imidazol-1-yl)phenyl)diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1-(4-nitrophenyl)-1H-imidazole (2301-25-9) → bis(4-(imidazol-1-yl)phenyl)diazene (1263305-79-8)

Guidance literature:

With sodium hydroxide; zinc; In water; isopropyl alcohol; for 24h; Reflux;

DOI:10.1021/ic102305v

Reference yield: 82.0%

bis(4-(imidazol-1-yl)phenyl)diazene (1263305-79-8) + magnesium meso-tetranitrooctaethylporphyrin (210413-94-8) → [Mg(meso-tetranitrooctaethylporphyrin(-2H))(NC3H3NC6H4NNC6H4NC3H3N)]

Guidance literature:

In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1021/ic300826p

Reference yield: 60.0%

cadmium(II) nitrate hexahydrate + bis(4-(imidazol-1-yl)phenyl)diazene (1263305-79-8) + oxybis(benzoic acid) (2215-89-6) → [Cd(bis-(4-imidazol-1-yl-phenyl)-diazene)(4,4'-oxybis(benzoate)(H2O)]n

Guidance literature:

In N,N-dimethyl-formamide; High Pressure; mixt. of diazene deriv., dicarboxylic acid, and Cd(NO3)2 in DMF stirred at room temp. for 32 h, soln. filtered, filtrate heated at 110°C in autoclave for 60 h, cooled to room temp. at 1°C/min; elem. anal.;

DOI:10.1016/j.poly.2009.09.005

upstream raw materials:

1-(4-nitrophenyl)-1H-imidazole

Downstream raw materials:

[Cd(bis-(4-imidazol-1-yl-phenyl)-diazene)(1,3-bis-(4'-carboxylatephenoxy)benzene)]n