methyl 1,4-epoxy-1,2,3,4-tetrahydro-1-phenyl-2-endo-phenanthrenecarboxylate

Base Information

Chemical Name:methyl 1,4-epoxy-1,2,3,4-tetrahydro-1-phenyl-2-endo-phenanthrenecarboxylate
CAS No.:114468-90-5
Molecular Formula:C₂₂H₁₈O₃
Molecular Weight:330.383
Hs Code.:

Synonyms:methyl 1,4-epoxy-1,2,3,4-tetrahydro-1-phenyl-2-endo-phenanthrenecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 1,4-epoxy-1,2,3,4-tetrahydro-1-phenyl-2-endo-phenanthrenecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of methyl 1,4-epoxy-1,2,3,4-tetrahydro-1-phenyl-2-endo-phenanthrenecarboxylate

There total 3 articles about methyl 1,4-epoxy-1,2,3,4-tetrahydro-1-phenyl-2-endo-phenanthrenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 114468-87-0
1-amino-1,3-dihydro-1-phenylnaphto<1,2-c>furan

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 114468-90-5
methyl 1,4-epoxy-1,2,3,4-tetrahydro-1-phenyl-2-endo-phenanthrenecarboxylate

Guidance literature:: With trichloroacetic acid; In toluene; for 10h; Heating;
DOI:10.1021/jo00248a009

Reference yield:

: 76635-70-6
(1-bromo-2-naphthyl)methanol

: 114468-90-5
methyl 1,4-epoxy-1,2,3,4-tetrahydro-1-phenyl-2-endo-phenanthrenecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

2: 79 percent / trichloroacetic acid / toluene / 10 h / Heating

With trichloroacetic acid; In toluene;
DOI:10.1021/jo00248a009

Reference yield:

: 100-47-0
benzonitrile

: 114468-90-5
methyl 1,4-epoxy-1,2,3,4-tetrahydro-1-phenyl-2-endo-phenanthrenecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

2: 79 percent / trichloroacetic acid / toluene / 10 h / Heating

With trichloroacetic acid; In toluene;
DOI:10.1021/jo00248a009