N-(4-bromomethyl-3-methoxybenzoyl)-2-methylbenzene sulfonamide

Base Information

• Chemical Name: N-(4-bromomethyl-3-methoxybenzoyl)-2-methylbenzene sulfonamide
• CAS No.: 1414930-95-2
• Molecular Formula: C₁₆H₁₆BrNO₄S
• Molecular Weight: 398.277
• Mol file: 1414930-95-2.mol

Synonyms:N-(4-bromomethyl-3-methoxybenzoyl)-2-methylbenzene sulfonamide

Chemical Property of N-(4-bromomethyl-3-methoxybenzoyl)-2-methylbenzene sulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N-(4-bromomethyl-3-methoxybenzoyl)-2-methylbenzene sulfonamide

There total 1 articles about N-(4-bromomethyl-3-methoxybenzoyl)-2-methylbenzene sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.3%

3-methoxy-4-methyl-N-(o-tolylsulfonyl) Benzamide (1414930-94-1) → N-(4-bromomethyl-3-methoxybenzoyl)-2-methylbenzene sulfonamide (1414930-95-2)

Guidance literature:

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile); In chloroform; at 60 - 65 ℃;

DOI:10.1080/00397911.2011.603875

Reference yield:

cyclopentyl-N-(1-methyl-1H-indol-5-yl)carbamate + N-(4-bromomethyl-3-methoxybenzoyl)-2-methylbenzene sulfonamide (1414930-95-2) → ZAFIRLUKAST (107753-78-6)

Guidance literature:

With silver(l) oxide; In 1,4-dioxane; at 20 - 100 ℃;

DOI:10.1080/00397911.2011.603875

upstream raw materials:

3-methoxy-4-methyl-N-(o-tolylsulfonyl) Benzamide

Downstream raw materials:

ZAFIRLUKAST