Technology Process of C25H23N3O6
There total 8 articles about C25H23N3O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hydroxide;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 1h;
regioselective reaction;
DOI:10.1016/j.ejmech.2013.01.002
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium tetrahydroborate / methanol / 1 h
2.1: triethylamine / dichloromethane / 2 h / 20 °C
3.1: ammonium acetate / ethanol / 24 h / 20 °C
3.2: 24 h / 20 °C
3.3: 0.5 h
4.1: lithium hydroxide / methanol; tetrahydrofuran / 1 h / 20 °C
With
sodium tetrahydroborate; ammonium acetate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
3.1: |Pinner Imino Ether Synthesis;
DOI:10.1016/j.ejmech.2013.01.002
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 48.5 h / 0 °C / Inert atmosphere; Reflux
2.1: palladium 10% on activated carbon; sodium tetrahydroborate / methanol / 1 h / 20 °C / 18751.9 Torr
3.1: methanol / 12 h / 20 °C / Molecular sieve; Inert atmosphere
4.1: sodium tetrahydroborate / methanol / 1 h
5.1: triethylamine / dichloromethane / 2 h / 20 °C
6.1: ammonium acetate / ethanol / 24 h / 20 °C
6.2: 24 h / 20 °C
6.3: 0.5 h
7.1: lithium hydroxide / methanol; tetrahydrofuran / 1 h / 20 °C
With
sodium tetrahydroborate; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; ammonium acetate; triethylamine; triphenylphosphine; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
1.1: |Mitsunobu Displacement / 6.1: |Pinner Imino Ether Synthesis;
DOI:10.1016/j.ejmech.2013.01.002
