(S)-(2-benzyloxy-pent-4-enyl)carbamoylmethyl-carbamic acid benzyl ester

Base Information

Chemical Name:(S)-(2-benzyloxy-pent-4-enyl)carbamoylmethyl-carbamic acid benzyl ester
CAS No.:1431373-85-1
Molecular Formula:C₂₂H₂₆N₂O₄
Molecular Weight:382.459
Hs Code.:

Synonyms:(S)-(2-benzyloxy-pent-4-enyl)carbamoylmethyl-carbamic acid benzyl ester

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Chemical Property of (S)-(2-benzyloxy-pent-4-enyl)carbamoylmethyl-carbamic acid benzyl ester

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Technology Process of (S)-(2-benzyloxy-pent-4-enyl)carbamoylmethyl-carbamic acid benzyl ester

There total 6 articles about (S)-(2-benzyloxy-pent-4-enyl)carbamoylmethyl-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1431373-84-0
?(S)-2-(2-benzyloxy-pent-4-enylamino)acetamide

: 501-53-1,94274-21-2
benzyl chloroformate

: 1431373-85-1
(S)-(2-benzyloxy-pent-4-enyl)carbamoylmethyl-carbamic acid benzyl ester

Guidance literature:: With sodium hydrogencarbonate; In ethanol; water; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.03.035

Reference yield:

: 79364-35-5
(S)-1-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)but-3-en-1-ol

: 1431373-85-1
(S)-(2-benzyloxy-pent-4-enyl)carbamoylmethyl-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C / Inert atmosphere

1.2: 14 h / 0 - 20 °C / Inert atmosphere

2.1: acetic acid / 24 h / 20 °C / Inert atmosphere

3.1: sodium periodate / water; methanol / 2 h / 20 °C / Inert atmosphere

4.1: triethylamine / methanol; diethyl ether / 0.17 h / 0 °C / Inert atmosphere

5.1: sodium cyanoborohydride / methanol; diethyl ether / 4 h / 0 - 20 °C / Inert atmosphere

6.1: sodium hydrogencarbonate / ethanol; water / 3 h / 0 - 20 °C / Inert atmosphere

With sodium periodate; sodium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; triethylamine; In methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tetlet.2013.03.035

Reference yield:

: 87604-53-3
(R)-4-((S)-1-(benzyloxy)but-3-ene-1-yl)-2,2-dimethyl-1,3-dioxypentane

: 1431373-85-1
(S)-(2-benzyloxy-pent-4-enyl)carbamoylmethyl-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / 24 h / 20 °C / Inert atmosphere

2: sodium periodate / water; methanol / 2 h / 20 °C / Inert atmosphere

3: triethylamine / methanol; diethyl ether / 0.17 h / 0 °C / Inert atmosphere

4: sodium cyanoborohydride / methanol; diethyl ether / 4 h / 0 - 20 °C / Inert atmosphere

5: sodium hydrogencarbonate / ethanol; water / 3 h / 0 - 20 °C / Inert atmosphere

With sodium periodate; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; triethylamine; In methanol; diethyl ether; ethanol; water;
DOI:10.1016/j.tetlet.2013.03.035