imidazole-1-carboxylic acid {5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide

Base Information

• Chemical Name: imidazole-1-carboxylic acid {5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide
• CAS No.: 1163706-68-0
• Molecular Formula: C₁₉H₁₄Cl₂N₆OS
• Molecular Weight: 445.332

Synonyms:imidazole-1-carboxylic acid {5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide

Chemical Property of imidazole-1-carboxylic acid {5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide

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Technology Process of imidazole-1-carboxylic acid {5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide

There total 1 articles about imidazole-1-carboxylic acid {5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-ylamine (1163706-69-1) + 1,1'-carbonyldiimidazole (530-62-1) → imidazole-1-carboxylic acid {5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide (1163706-68-0)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 18h;

Reference yield:

imidazole-1-carboxylic acid {5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide (1163706-68-0) + (2S,3S)-3-methyl-pyrrolidine-2-carboxylic acid amide (76260-81-6) → (2S,3S)-3-methyl-pyrrolidine-1,2-dicarboxylic acid 2-amide 1-({5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide) (1163705-15-4)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 40 ℃; for 18h;

Reference yield:

imidazole-1-carboxylic acid {5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide (1163706-68-0) + (S)-2-methylpyrrolidine-2-carboxylic acid amide (132235-43-9) → (S)-2-methyl-pyrrolidine-1,2-dicarboxylic acid 2-amide 1-({5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide) (1163705-29-0)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 40 ℃; for 18h;

upstream raw materials:

5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-ylamine

1,1'-carbonyldiimidazole

Downstream raw materials:

(2S,3S)-3-methyl-pyrrolidine-1,2-dicarboxylic acid 2-amide 1-({5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide)

(S)-2-methyl-pyrrolidine-1,2-dicarboxylic acid 2-amide 1-({5-[2-(2,6-dichloro-benzyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-yl}-amide)

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