C₁₉H₂₉⁽²⁾HSi

Base Information

Chemical Name:C₁₉H₂₉⁽²⁾HSi
CAS No.:253448-39-4
Molecular Formula:C₁₉H₃₀Si
Molecular Weight:287.525
Hs Code.:

C<sub>19</sub>H<sub>29</sub><sup>(2)</sup>HSi

Synonyms:C₁₉H₂₉⁽²⁾HSi

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Chemical Property of C₁₉H₂₉⁽²⁾HSi

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Technology Process of C₁₉H₂₉⁽²⁾HSi

There total 5 articles about C₁₉H₂₉⁽²⁾HSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 2170-06-1
1-Phenyl-2-(trimethylsilyl)acetylene

: 253448-37-2
(Z)-(S)-1-Iodo-3,4,4-trimethyl-pent-1-ene

: 253448-39-4
C₁₉H₂₉⁽²⁾HSi

Guidance literature:: 1-Phenyl-2-(trimethylsilyl)acetylene; With bis(cyclopentadienyl)titanium dichloride; isobutylmagnesium bromide; zinc(II) chloride; In tetrahydrofuran;

(Z)-(S)-1-Iodo-3,4,4-trimethyl-pent-1-ene; With tetrakis(triphenylphosphine) palladium⁽⁰⁾;
DOI:10.1021/ja992498e

Reference yield:

: 13332-16-6
(R)-2,3,3-Trimethyl-1-butanol

: 253448-39-4
C₁₉H₂₉⁽²⁾HSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: PCC / CH₂Cl₂

2.1: 65 percent / NaHMDS / tetrahydrofuran / -78 °C

3.1: [2-2H₁]-iBuMgBr; Cp₂TiCl₂; ZnCl₂ / tetrahydrofuran

3.2: 67 percent / Pd(PPh₃)4

With bis(cyclopentadienyl)titanium dichloride; isobutylmagnesium bromide; sodium hexamethyldisilazane; pyridinium chlorochromate; zinc(II) chloride; In tetrahydrofuran; dichloromethane; 1.1: Oxidation / 2.1: Wittig olefination / 3.1: Substitution / 3.2: Condensation;
DOI:10.1021/ja992498e

Reference yield:

: 96930-22-2
(4R,5S)-3-(3,3-Dimethyl-butyryl)-4-methyl-5-phenyl-oxazolidin-2-one

: 253448-39-4
C₁₉H₂₉⁽²⁾HSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaHMDS / tetrahydrofuran / 2 h / -78 °C

1.2: 77 percent / tetrahydrofuran

2.1: BnSH; BnSLi / tetrahydrofuran / 0 °C

2.2: LAH / tetrahydrofuran

3.1: PCC / CH₂Cl₂

4.1: 65 percent / NaHMDS / tetrahydrofuran / -78 °C

5.1: [2-2H₁]-iBuMgBr; Cp₂TiCl₂; ZnCl₂ / tetrahydrofuran

5.2: 67 percent / Pd(PPh₃)4

With bis(cyclopentadienyl)titanium dichloride; isobutylmagnesium bromide; sodium hexamethyldisilazane; lithium phenylmethanethiolate; phenylmethanethiol; pyridinium chlorochromate; zinc(II) chloride; In tetrahydrofuran; dichloromethane; 1.1: Metallation / 1.2: Methylation / 2.1: Ring cleavage / 2.2: Reduction / 3.1: Oxidation / 4.1: Wittig olefination / 5.1: Substitution / 5.2: Condensation;
DOI:10.1021/ja992498e