4,5-dihydro-1,2,9,10-tetramethoxy-7-(phenylmethoxy)-6H-dibenzoquinoline

Base Information

Chemical Name:4,5-dihydro-1,2,9,10-tetramethoxy-7-(phenylmethoxy)-6H-dibenzoquinoline
CAS No.:116103-68-5
Molecular Formula:C₂₇H₂₇NO₅
Molecular Weight:445.515
Hs Code.:

4,5-dihydro-1,2,9,10-tetramethoxy-7-(phenylmethoxy)-6H-dibenzo<de,g>quinoline

Synonyms:4,5-dihydro-1,2,9,10-tetramethoxy-7-(phenylmethoxy)-6H-dibenzoquinoline

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Chemical Property of 4,5-dihydro-1,2,9,10-tetramethoxy-7-(phenylmethoxy)-6H-dibenzoquinoline

Chemical Property:

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Technology Process of 4,5-dihydro-1,2,9,10-tetramethoxy-7-(phenylmethoxy)-6H-dibenzoquinoline

There total 4 articles about 4,5-dihydro-1,2,9,10-tetramethoxy-7-(phenylmethoxy)-6H-dibenzoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 116103-67-4
ethyl 7-(benzyloxy)-1,2,9,10-tetramethoxy-6a,7-didehydronoraporphine-6-carboxylate

: 116103-68-5
4,5-dihydro-1,2,9,10-tetramethoxy-7-(phenylmethoxy)-6H-dibenzoquinoline

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In benzene; for 18h; Ambient temperature;
DOI:10.1021/jo00254a005

Reference yield:

: 100-39-0
benzyl bromide

: 116103-68-5
4,5-dihydro-1,2,9,10-tetramethoxy-7-(phenylmethoxy)-6H-dibenzoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / potassium carbonate / acetone / 6 h / Heating

2: 80 percent / sodium bis(methoxyethoxy)aluminum hydride / benzene / 18 h / Ambient temperature

With potassium carbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; In acetone; benzene;
DOI:10.1021/jo00254a005

Reference yield:

: 116103-66-3
ethyl 4,5-dihydro-7-hydroxy-1,2,9,10-tetramethoxy-6H-dibenzoquinoline-6-carboxylate

: 116103-68-5
4,5-dihydro-1,2,9,10-tetramethoxy-7-(phenylmethoxy)-6H-dibenzoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / potassium carbonate / acetone / 6 h / Heating

2: 80 percent / sodium bis(methoxyethoxy)aluminum hydride / benzene / 18 h / Ambient temperature

With potassium carbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; In acetone; benzene;
DOI:10.1021/jo00254a005