C₂₉H₂₇NO₆S

Base Information

Chemical Name:C₂₉H₂₇NO₆S
CAS No.:1472655-14-3
Molecular Formula:C₂₉H₂₇NO₆S
Molecular Weight:517.602
Hs Code.:

C<sub>29</sub>H<sub>27</sub>NO<sub>6</sub>S

Synonyms:C₂₉H₂₇NO₆S

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Chemical Property of C₂₉H₂₇NO₆S

Chemical Property:

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Technology Process of C₂₉H₂₇NO₆S

There total 5 articles about C₂₉H₂₇NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1360958-86-6
C₈H₇NOS

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 1472655-14-3
C₂₉H₂₇NO₆S

Guidance literature:: C₈H₇NOS; With N,O-bis-(trimethylsilyl)-acetamide; In dichloromethane; at 20 ℃; for 0.666667h; Inert atmosphere;

2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride; With tin(IV) chloride; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja408814g

Reference yield:

: 1585965-73-6
C₈H₇N₃OS

: 1472655-14-3
C₂₉H₂₇NO₆S

Guidance literature:: Multi-step reaction with 2 steps

1.1: chloroform; diphenylether / 1 h / 230 °C

2.1: N,O-bis-(trimethylsilyl)-acetamide / dichloromethane / 0.67 h / 20 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With N,O-bis-(trimethylsilyl)-acetamide; In diphenylether; dichloromethane; chloroform; 1.1: |Curtius Rearrangement;
DOI:10.1021/ja408814g

Reference yield:

: 29421-72-5
2-methyl-4-thiophenecarboxaldehyde

: 1472655-14-3
C₂₉H₂₇NO₆S

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine; piperidine / 13 h / 100 °C

2.1: thionyl chloride / chloroform; N,N-dimethyl-formamide / 3 h / Reflux

3.1: sodium azide / 1,4-dioxane; water / 0.5 h / 5 °C

4.1: chloroform; diphenylether / 1 h / 230 °C

5.1: N,O-bis-(trimethylsilyl)-acetamide / dichloromethane / 0.67 h / 20 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

With piperidine; pyridine; thionyl chloride; sodium azide; N,O-bis-(trimethylsilyl)-acetamide; In 1,4-dioxane; diphenylether; dichloromethane; chloroform; water; N,N-dimethyl-formamide; 4.1: |Curtius Rearrangement;
DOI:10.1021/ja408814g