ethyl 2-(4-(3-(4-amino-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

Base Information

Chemical Name:ethyl 2-(4-(3-(4-amino-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate
CAS No.:1269425-33-3
Molecular Formula:C₂₅H₃₅NO₄S
Molecular Weight:445.623
Hs Code.:

Synonyms:ethyl 2-(4-(3-(4-amino-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

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Chemical Property of ethyl 2-(4-(3-(4-amino-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

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Technology Process of ethyl 2-(4-(3-(4-amino-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

There total 5 articles about ethyl 2-(4-(3-(4-amino-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1269425-31-1
ethyl 2-(4-(3-(4-(tert-butoxycarbonylamino)-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

: 1269425-33-3
ethyl 2-(4-(3-(4-amino-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/ardp.201000091

Reference yield:

: 1186435-67-5
ethyl 2-(4-hydroxyphenylthio)hexanoate

: 1269425-33-3
ethyl 2-(4-(3-(4-amino-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 60 h / Reflux

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C / Cooling with ice; Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With potassium carbonate; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; acetonitrile; 1: Williamson-like ether synthesis / 2: Mitsunobu reaction;
DOI:10.1002/ardp.201000091

Reference yield:

: 1186435-44-8
ethyl 2-(4-(3-hydroxypropoxy)phenylthio)hexanoate

: 1269425-33-3
ethyl 2-(4-(3-(4-amino-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C / Cooling with ice; Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 1: Mitsunobu reaction;
DOI:10.1002/ardp.201000091