ethyl 2-(4-(3-(4-(tert-butoxycarbonylamino)-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

Base Information

Chemical Name:ethyl 2-(4-(3-(4-(tert-butoxycarbonylamino)-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate
CAS No.:1269425-31-1
Molecular Formula:C₃₀H₄₃NO₆S
Molecular Weight:545.741
Hs Code.:

Synonyms:ethyl 2-(4-(3-(4-(tert-butoxycarbonylamino)-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

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Chemical Property of ethyl 2-(4-(3-(4-(tert-butoxycarbonylamino)-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

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Technology Process of ethyl 2-(4-(3-(4-(tert-butoxycarbonylamino)-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

There total 4 articles about ethyl 2-(4-(3-(4-(tert-butoxycarbonylamino)-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 224450-47-9
(4-hydroxy-2,3-dimethylphenyl)carbamic acid tert-butyl ester

: 1186435-44-8
ethyl 2-(4-(3-hydroxypropoxy)phenylthio)hexanoate

: 1269425-31-1
ethyl 2-(4-(3-(4-(tert-butoxycarbonylamino)-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; Cooling with ice; Inert atmosphere;
DOI:10.1002/ardp.201000091

Reference yield:

: 1186435-67-5
ethyl 2-(4-hydroxyphenylthio)hexanoate

: 1269425-31-1
ethyl 2-(4-(3-(4-(tert-butoxycarbonylamino)-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 60 h / Reflux

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C / Cooling with ice; Inert atmosphere

With potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; acetonitrile; 1: Williamson-like ether synthesis / 2: Mitsunobu reaction;
DOI:10.1002/ardp.201000091

Reference yield:

: 637-89-8
4-sulfanylphenol

: 1269425-31-1
ethyl 2-(4-(3-(4-(tert-butoxycarbonylamino)-2,3-dimethylphenoxy)propoxy)phenylthio)hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / chloroform / 1.5 h / Reflux

2: potassium carbonate / acetonitrile / 60 h / Reflux

3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C / Cooling with ice; Inert atmosphere

With potassium carbonate; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; chloroform; acetonitrile; 2: Williamson-like ether synthesis / 3: Mitsunobu reaction;
DOI:10.1002/ardp.201000091