(E)-3-cyclohexylbut-2-enenitrile

Base Information

Chemical Name:(E)-3-cyclohexylbut-2-enenitrile
CAS No.:1638142-35-4
Molecular Formula:C₁₀H₁₅N
Molecular Weight:149.236
Hs Code.:

Synonyms:(E)-3-cyclohexylbut-2-enenitrile

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Chemical Property of (E)-3-cyclohexylbut-2-enenitrile

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Technology Process of (E)-3-cyclohexylbut-2-enenitrile

There total 6 articles about (E)-3-cyclohexylbut-2-enenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: C₁₀H₁₇NO

: 1638142-35-4
(E)-3-cyclohexylbut-2-enenitrile

Guidance literature:: With silver(I) acetate; lithium chloride; palladium dichloride; In acetonitrile; at 80 ℃; Inert atmosphere;
DOI:10.1021/jacs.5b06418

Reference yield:

: 823-76-7
Cyclohexyl methyl ketone

: 1638142-35-4
(E)-3-cyclohexylbut-2-enenitrile

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 1.5 h / 0 °C / Inert atmosphere

1.2: 4 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox

2.1: sodium hydroxide / ethanol / 20 °C / Inert atmosphere

3.1: thionyl chloride / Inert atmosphere; Reflux

4.1: ammonium hydroxide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

5.1: palladium dichloride; silver(I) acetate; lithium chloride / acetonitrile / 80 °C / Inert atmosphere

With ammonium hydroxide; thionyl chloride; silver(I) acetate; sodium hydride; lithium chloride; sodium hydroxide; palladium dichloride; In tetrahydrofuran; ethanol; acetonitrile; mineral oil;
DOI:10.1021/jacs.5b06418

Reference yield:

: 95979-82-1
(E)-3-cyclohexylbut-2-enoyl chloride

: 1638142-35-4
(E)-3-cyclohexylbut-2-enenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2: palladium dichloride; silver(I) acetate; lithium chloride / acetonitrile / 80 °C / Inert atmosphere

With ammonium hydroxide; silver(I) acetate; lithium chloride; palladium dichloride; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jacs.5b06418