ethyl 3-cyclohexylbut-2-enoate

Base Information

Chemical Name:ethyl 3-cyclohexylbut-2-enoate
CAS No.:28811-79-2
Molecular Formula:C₁₂H₂₀O₂
Molecular Weight:196.29
Hs Code.:

Synonyms:ethyl 3-cyclohexylbut-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 3-cyclohexylbut-2-enoate

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of ethyl 3-cyclohexylbut-2-enoate

There total 11 articles about ethyl 3-cyclohexylbut-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 4341-76-8
Ethyl 2-butynoate

: 931-51-1
cyclohexylmagnesiumchloride

: 28811-79-2,73232-03-8,73232-02-7
(E)-ethyl 3-cyclohexylbut-2-enoate

Guidance literature:: cyclohexylmagnesiumchloride; With copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at -78 - -40 ℃; for 0.5h;

Ethyl 2-butynoate; In tetrahydrofuran; at -78 ℃; for 4h;
DOI:10.1039/d0ob01315c

Reference yield: 83.0%

: 931-48-6
2-cyclohexylacetylene

: 75-24-1
trimethylaluminum

: 541-41-3
chloroformic acid ethyl ester

: 28811-79-2,73232-03-8,73232-02-7
(E)-ethyl 3-cyclohexylbut-2-enoate

Guidance literature:: 2-cyclohexylacetylene; trimethylaluminum; With zirconocene dichloride; In hexane; dichloromethane; at -23 - 20 ℃; Inert atmosphere;

chloroformic acid ethyl ester; In hexane; dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja2066219

Reference yield: 77.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 823-76-7
Cyclohexyl methyl ketone

: 28811-79-2,73232-03-8,73232-02-7
(E)-ethyl 3-cyclohexylbut-2-enoate

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.5h; Inert atmosphere;

Cyclohexyl methyl ketone; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.9b00729