2-(6-nitrooxy-hexanoyloxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

Base Information

Chemical Name:2-(6-nitrooxy-hexanoyloxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester
CAS No.:1240261-59-9
Molecular Formula:C₁₉H₂₄N₂O₁₂
Molecular Weight:472.406
Hs Code.:

Synonyms:2-(6-nitrooxy-hexanoyloxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

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Chemical Property of 2-(6-nitrooxy-hexanoyloxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

Chemical Property:

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Technology Process of 2-(6-nitrooxy-hexanoyloxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

There total 6 articles about 2-(6-nitrooxy-hexanoyloxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1240261-58-8
2-(6-bromo-hexanoyloxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

: 1240261-59-9
2-(6-nitrooxy-hexanoyloxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

Guidance literature:: With silver nitrate; In acetonitrile; at 20 ℃; for 20h;

Reference yield:

: 69-72-7,25496-36-0,8052-31-1
salicylic acid

: 1240261-59-9
2-(6-nitrooxy-hexanoyloxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / acetone / 4 h / 50 °C

2: hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h

3: triethylamine / acetone / 16 h / 40 °C

4: silver nitrate / acetonitrile / 8 h / 50 °C

5: pyridine / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

6: silver nitrate / acetonitrile / 20 h / 20 °C

With pyridine; hydrogen; silver nitrate; triethylamine; palladium 10% on activated carbon; In dichloromethane; ethyl acetate; acetone; acetonitrile;

Reference yield:

: 1240261-43-1
2-hydroxy-benzoic acid benzyloxy carbonyl methyl ester

: 1240261-59-9
2-(6-nitrooxy-hexanoyloxy)-benzoic acid 4-nitrooxy-butoxy carbonyl methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h

2: triethylamine / acetone / 16 h / 40 °C

3: silver nitrate / acetonitrile / 8 h / 50 °C

4: pyridine / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

5: silver nitrate / acetonitrile / 20 h / 20 °C

With pyridine; hydrogen; silver nitrate; triethylamine; palladium 10% on activated carbon; In dichloromethane; ethyl acetate; acetone; acetonitrile;