3-(2,5-dioxo-2H-pyrrol-1(5H)-yl)-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)benzyl)-N-methylpropanamide

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Chemical Name:3-(2,5-dioxo-2H-pyrrol-1(5H)-yl)-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)benzyl)-N-methylpropanamide
CAS No.:1321992-91-9
Molecular Formula:C₃₂H₄₆F₆N₂O₅Sn
Molecular Weight:771.428
Hs Code.:

Synonyms:3-(2,5-dioxo-2H-pyrrol-1(5H)-yl)-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)benzyl)-N-methylpropanamide

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Chemical Property of 3-(2,5-dioxo-2H-pyrrol-1(5H)-yl)-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)benzyl)-N-methylpropanamide

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Technology Process of 3-(2,5-dioxo-2H-pyrrol-1(5H)-yl)-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)benzyl)-N-methylpropanamide

There total 8 articles about 3-(2,5-dioxo-2H-pyrrol-1(5H)-yl)-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)benzyl)-N-methylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 55750-62-4
3-maleimidopropionic acid N-hydroxysuccinimide ester

: 1321992-88-4
(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)phenyl)-N-methylmethanamine

: 1321992-91-9
3-(2,5-dioxo-2H-pyrrol-1(5H)-yl)-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)benzyl)-N-methylpropanamide

Guidance literature:: In acetonitrile; at 20 ℃;

Reference yield:

: 1321992-74-8
2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodo-4-methylbenzene

: 1321992-91-9
3-(2,5-dioxo-2H-pyrrol-1(5H)-yl)-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)benzyl)-N-methylpropanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 15 h / 78 °C / Inert atmosphere

2.1: potassium carbonate; potassium iodide / acetonitrile / 40 °C / Inert atmosphere

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C

3.2: -78 - 20 °C

4.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 4 h / 35 °C / Inert atmosphere

5.1: acetonitrile / 20 °C

With N-Bromosuccinimide; n-butyllithium; 1,3-dimethylbarbituric acid; potassium carbonate; potassium iodide; dibenzoyl peroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; tetrachloromethane; hexane; dichloromethane; acetonitrile;

Reference yield:

: 1321992-80-6
4-(bromomethyl)-2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodobenzene

: 1321992-91-9
3-(2,5-dioxo-2H-pyrrol-1(5H)-yl)-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)benzyl)-N-methylpropanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; potassium iodide / acetonitrile / 40 °C / Inert atmosphere

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C

2.2: -78 - 20 °C

3.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 4 h / 35 °C / Inert atmosphere

4.1: acetonitrile / 20 °C

With n-butyllithium; 1,3-dimethylbarbituric acid; potassium carbonate; potassium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; dichloromethane; acetonitrile;