2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodo-4-methylbenzene

Base Information

Chemical Name:2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodo-4-methylbenzene
CAS No.:1321992-74-8
Molecular Formula:C₁₂H₁₁F₆IO₂
Molecular Weight:428.113
Hs Code.:

Synonyms:2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodo-4-methylbenzene

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Chemical Property of 2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodo-4-methylbenzene

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Technology Process of 2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodo-4-methylbenzene

There total 2 articles about 2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodo-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1992-07-0
4-methyl-2-<1-hydroxy-1-(trifluoromethyl)-2,2,2-trifluoroethyl>aniline

: 1321992-74-8
2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodo-4-methylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; sulfuric acid / water / 0 °C

1.2: 80 °C / Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / 20 °C / Cooling with ice

With sulfuric acid; N-ethyl-N,N-diisopropylamine; sodium nitrite; In water;

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 1321992-74-8
2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodo-4-methylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / chlorobenzene; water / 5 h / 100 °C

2.1: sodium nitrite; sulfuric acid / water / 0 °C

2.2: 80 °C / Cooling with ice

3.1: N-ethyl-N,N-diisopropylamine / 20 °C / Cooling with ice

With sulfuric acid; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; sodium nitrite; In water; chlorobenzene;