3-(1,1-Dioxo-4-phenylsulfanyl-2,5-dihydro-1H-1λ⁶-thiophen-2-yl)-propionaldehyde

Base Information

Chemical Name:3-(1,1-Dioxo-4-phenylsulfanyl-2,5-dihydro-1H-1λ⁶-thiophen-2-yl)-propionaldehyde
CAS No.:197862-45-6
Molecular Formula:C₁₃H₁₄O₃S₂
Molecular Weight:282.384
Hs Code.:

3-(1,1-Dioxo-4-phenylsulfanyl-2,5-dihydro-1H-1λ<sup>6</sup>-thiophen-2-yl)-propionaldehyde

Synonyms:3-(1,1-Dioxo-4-phenylsulfanyl-2,5-dihydro-1H-1λ⁶-thiophen-2-yl)-propionaldehyde

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Chemical Property of 3-(1,1-Dioxo-4-phenylsulfanyl-2,5-dihydro-1H-1λ⁶-thiophen-2-yl)-propionaldehyde

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Technology Process of 3-(1,1-Dioxo-4-phenylsulfanyl-2,5-dihydro-1H-1λ⁶-thiophen-2-yl)-propionaldehyde

There total 2 articles about 3-(1,1-Dioxo-4-phenylsulfanyl-2,5-dihydro-1H-1λ⁶-thiophen-2-yl)-propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 197862-43-4
3-(1,1-Dioxo-4-phenylsulfanyl-2,5-dihydro-1H-1λ⁶-thiophen-2-yl)-propan-1-ol

: 197862-45-6
3-(1,1-Dioxo-4-phenylsulfanyl-2,5-dihydro-1H-1λ⁶-thiophen-2-yl)-propionaldehyde

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1002/jccs.199700055

Reference yield:

: 110026-88-5
2-Allyl-4-phenylsulfanyl-2,5-dihydro-thiophene 1,1-dioxide

: 197862-45-6
3-(1,1-Dioxo-4-phenylsulfanyl-2,5-dihydro-1H-1λ⁶-thiophen-2-yl)-propionaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 9-borabicyclo<3.3.1>nonane, 2.) aq. NaOH, 30percent aq. H₂O₂ / 1.) THF, from 0 deg C to RT, 2.) THF, from 0 deg C to RT

2: 80 percent / pyridinium chlorochromate / CH₂Cl₂ / 3 h / Ambient temperature

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; pyridinium chlorochromate; In dichloromethane;
DOI:10.1002/jccs.199700055