N^α-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-N^ε-benzyloxycarbonyl-L-lysine

Base Information

• Chemical Name: N^α-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-N^ε-benzyloxycarbonyl-L-lysine
• CAS No.: 129297-31-0
• Molecular Formula: C₃₆H₅₁N₃O₈
• Molecular Weight: 653.816

Synonyms:N^α-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-N^ε-benzyloxycarbonyl-L-lysine

Chemical Property of N^α-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-N^ε-benzyloxycarbonyl-L-lysine

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Technology Process of N^α-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-N^ε-benzyloxycarbonyl-L-lysine

There total 6 articles about N^α-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-N^ε-benzyloxycarbonyl-L-lysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Nα-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-Nε-benzyloxycarbonyl-L-lysine tert-butyl ester (120008-84-6) → Nα-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-Nε-benzyloxycarbonyl-L-lysine (129297-31-0)

Guidance literature:

With formic acid; at 40 ℃; for 30h;

Reference yield:

Nα-<1(R)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-Nε-benzyloxycarbonyl-L-lysine tert-butyl ester (129388-76-7) → 4-[(R)-6-((S)-5-Benzyloxycarbonylamino-1-carboxy-pentylamino)-6-ethoxycarbonyl-hexyl]-piperidine-1-carboxylic acid benzyl ester (129297-31-0)

Guidance literature:

With formic acid; at 40 ℃; for 30h;

Reference yield:

Nε-benzyloxycarbonyl-L-lysine tert-butyl ester (63628-63-7) → Nα-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-Nε-benzyloxycarbonyl-L-lysine (129297-31-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 44 percent / Et₃N, KI / acetonitrile / 72 h / Heating

2: 85 percent / 99percent formic acid / 30 h / 40 °C

With formic acid; triethylamine; potassium iodide; In acetonitrile;

upstream raw materials:

N^α-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-N^ε-benzyloxycarbonyl-L-lysine tert-butyl ester

Nε-benzyloxycarbonyl-L-lysine tert-butyl ester

ethyl 7-(1-benzyloxycarbonyl-4-piperidyl)-2-chloroheptanoate

N^α-<1(R)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-N^ε-benzyloxycarbonyl-L-lysine tert-butyl ester

Downstream raw materials:

4-{(R)-6-[(S)-5-Benzyloxycarbonylamino-1-((S)-2-tert-butoxycarbonyl-pyrrolidine-1-carbonyl)-pentylamino]-6-ethoxycarbonyl-hexyl}-piperidine-1-carboxylic acid benzyl ester

N^α-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-N^ε-benzyloxycarbonyl-L-lysyl-L-proline tert-butyl ester

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