bis(tetraphenylphosphonium) hexakis(μ-thiophenolato)-tetrachlorotetraferrate(II)

Base Information

Chemical Name:bis(tetraphenylphosphonium) hexakis(μ-thiophenolato)-tetrachlorotetraferrate(II)
CAS No.:80765-11-3
Molecular Formula:2C₂₄H₂₀P*C₃₆H₃₀Cl₄Fe₄S₆
Molecular Weight:1699.02
Hs Code.:

Synonyms:bis(tetraphenylphosphonium) hexakis(μ-thiophenolato)-tetrachlorotetraferrate(II)

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Chemical Property of bis(tetraphenylphosphonium) hexakis(μ-thiophenolato)-tetrachlorotetraferrate(II)

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Technology Process of bis(tetraphenylphosphonium) hexakis(μ-thiophenolato)-tetrachlorotetraferrate(II)

There total 1 articles about bis(tetraphenylphosphonium) hexakis(μ-thiophenolato)-tetrachlorotetraferrate(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3111-52-2
potassium thiophenolate

: 2001-45-8
tetraphenyl phosphonium chloride

: iron(II) chloride

: 80765-11-3
bis(tetraphenylphosphonium) hexakis(μ-thiophenolato)-tetrachlorotetraferrate(II)

Guidance literature:: (N2);
DOI:10.1021/ja00371a016

Reference yield: 84.0%

: 80765-11-3
bis(tetraphenylphosphonium) hexakis(μ-thiophenolato)-tetrachlorotetraferrate(II)

: 6493-73-8
dibenzyltrisulfide

: 80939-30-6
bis(tetraphenylphosphonium) bis(thiophenolato)dichlorotetrakis(μ3-sulfido)tetraferrate(2II,2III)

Guidance literature:: In acetonitrile; soln. of dibenzyltrisufide was added to soln. of complex (mol ratio 4:1) (N2); stirring for 20 min; addn. of EtOH/Et2O, standing for ca 2 h; elem. anal.;
DOI:10.1021/ja00371a016

Reference yield: 73.0%

: 80765-11-3
bis(tetraphenylphosphonium) hexakis(μ-thiophenolato)-tetrachlorotetraferrate(II)

: 6493-73-8
dibenzyltrisulfide

: bis(tetraphenylphosphonium) tetrachlorotetrakis(μ3-sulfido)tetraferrate(2II,2III)

Guidance literature:: In acetonitrile; soln. of trisulfide was added to soln. of complex (mol ratio 8:1) (N2);stirring for 15 min; filtration, addn. of Et2O, standing for ca 5 h, crystals isolation, washing with Et2O, drying; recrystn. from DMF/Et2O;
DOI:10.1021/ja00371a016