[Cp*Ru(C_.ident.CC(CH₂NO₂)Ph₂)(PEt₃)2]

Base Information

• Chemical Name: [Cp*Ru(C_.ident.CC(CH₂NO₂)Ph₂)(PEt₃)2]
• CAS No.: 1124379-40-3
• Molecular Formula: C₃₈H₅₇NO₂P₂Ru
• Molecular Weight: 722.894

Synonyms:[Cp*Ru(C_.ident.CC(CH₂NO₂)Ph₂)(PEt₃)2]

Chemical Property of [Cp*Ru(C_.ident.CC(CH₂NO₂)Ph₂)(PEt₃)2]

Chemical Property:

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Technology Process of [Cp*Ru(C_.ident.CC(CH₂NO₂)Ph₂)(PEt₃)2]

There total 1 articles about [Cp*Ru(C_.ident.CC(CH₂NO₂)Ph₂)(PEt₃)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

nitromethane (75-52-5) + [Cp*Ru(=C=C=CPh2)(PEt3)2][BF4] → [Cp*Ru(C.ident.CC(CH2NO2)Ph2)(PEt3)2] (1124379-40-3)

Guidance literature:

With (CH₃)3COK; In tetrahydrofuran; (N2 or Ar); addn. of a suspn. of (t)BuOK and nitromethane in THF to a soln. of Ru complex in THF, stirring for 30 min; evapn. in vac., extn. with petroleum ether, filtration through Celite, evapn. in vac.; elem. anal.;

DOI:10.1021/om801125f

Reference yield: 81.0%

tetrafluoroboric acid diethyl ether (67969-82-8) + [Cp*Ru(C.ident.CC(CH2NO2)Ph2)(PEt3)2] (1124379-40-3) → [Cp*Ru(=C=CHC(CH2NO2)Ph2)(PEt3)2][BF4]

Guidance literature:

In diethyl ether; (N2 or Ar); addn. of a soln. of acid in Et2O to a soln. of Ru complex inEt2O cooled in ethanol/liquid N2 bath, warming to room temp. with stirr ing; evapn. in vac., extn. with CH2Cl2, filtration through Celite, evapn. in vac., washing with Et2O; elem. anal.;

DOI:10.1021/om801125f

upstream raw materials:

nitromethane

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