O-(2-Azido-4,6-O-benzyliden-2-desoxy-α-D-galactopyranosyl)trichloracetimidat

Base Information

Chemical Name:O-(2-Azido-4,6-O-benzyliden-2-desoxy-α-D-galactopyranosyl)trichloracetimidat
CAS No.:94715-44-3
Molecular Formula:C₁₅H₁₅Cl₃N₄O₅
Molecular Weight:437.667
Hs Code.:

Synonyms:O-(2-Azido-4,6-O-benzyliden-2-desoxy-α-D-galactopyranosyl)trichloracetimidat

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Chemical Property of O-(2-Azido-4,6-O-benzyliden-2-desoxy-α-D-galactopyranosyl)trichloracetimidat

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Technology Process of O-(2-Azido-4,6-O-benzyliden-2-desoxy-α-D-galactopyranosyl)trichloracetimidat

There total 5 articles about O-(2-Azido-4,6-O-benzyliden-2-desoxy-α-D-galactopyranosyl)trichloracetimidat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 2-Azido-4,6-O-benzyliden-2-desoxy-D-galactopyranose

: 545-06-2
trichloroacetonitrile

: 94715-44-3
O-(2-Azido-4,6-O-benzyliden-2-desoxy-α-D-galactopyranosyl)trichloracetimidat

: O-(2-Azido-4,6-O-benzyliden-2-desoxy-3-O-trichloracetimidoyl-α-D-galactopyranosyl)trichloracetimidat

Guidance literature:: With sodium hydride; In 1,2-dimethoxyethane; for 2h;

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 94715-44-3
O-(2-Azido-4,6-O-benzyliden-2-desoxy-α-D-galactopyranosyl)trichloracetimidat

Guidance literature:: Multi-step reaction with 2 steps

1: 6 percent / p-toluenesulphonic acid / dimethylformamide / 5 h / 50 °C

2: 64 percent / NaH / 1,2-dimethoxy-ethane / 2 h

With sodium hydride; toluene-4-sulfonic acid; In 1,2-dimethoxyethane; N,N-dimethyl-formamide;

Reference yield:

: 3,4,6-tri-O-acetyl-2-azido-2-deoxy-D-lyxo-hexopyranose

: 94715-44-3
O-(2-Azido-4,6-O-benzyliden-2-desoxy-α-D-galactopyranosyl)trichloracetimidat

Guidance literature:: Multi-step reaction with 5 steps

1: 69 percent / imidazole / dimethylformamide / 4 h / Ambient temperature

2: 88 percent / CH₃OH/Na / 18 h / Ambient temperature

3: 78 percent / p-toluenesulphonic acid / dimethylformamide / 5 h / 50 °C

4: 61 percent / tetrabutylammoniumfluoride / CH₂Cl₂ / 7 h / Ambient temperature

5: 64 percent / NaH / 1,2-dimethoxy-ethane / 2 h

With 1H-imidazole; methanol; tetrabutyl ammonium fluoride; sodium; sodium hydride; toluene-4-sulfonic acid; In 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide;