tert-Butyldimethylsilyl-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

Base Information

Chemical Name:tert-Butyldimethylsilyl-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid
CAS No.:87190-68-9
Molecular Formula:C₁₉H₂₉N₃O₅Si
Molecular Weight:407.542
Hs Code.:

Synonyms:tert-Butyldimethylsilyl-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

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Chemical Property of tert-Butyldimethylsilyl-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

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Technology Process of tert-Butyldimethylsilyl-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

There total 4 articles about tert-Butyldimethylsilyl-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 94715-52-3
tert-butyldimethylsilyl-2-azido-2-desoxy-β-D-galactopyranosid

: 2-Azido-4,6-O-benzyliden-2-desoxy-D-galactopyranose

: 87190-68-9
tert-Butyldimethylsilyl-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 50 ℃; for 5h;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 87190-68-9
tert-Butyldimethylsilyl-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / imidazole / dimethylformamide / 4 h / Ambient temperature

2: 88 percent / CH₃OH/Na / 18 h / Ambient temperature

3: 78 percent / p-toluenesulphonic acid / dimethylformamide / 5 h / 50 °C

With 1H-imidazole; methanol; sodium; toluene-4-sulfonic acid; In N,N-dimethyl-formamide;

Reference yield:

: 3,4,6-tri-O-acetyl-2-azido-2-deoxy-D-lyxo-hexopyranose

: 87190-68-9
tert-Butyldimethylsilyl-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / imidazole / dimethylformamide / 4 h / Ambient temperature

2: 88 percent / CH₃OH/Na / 18 h / Ambient temperature

3: 78 percent / p-toluenesulphonic acid / dimethylformamide / 5 h / 50 °C

With 1H-imidazole; methanol; sodium; toluene-4-sulfonic acid; In N,N-dimethyl-formamide;