((S)-2-{3-[1-(3-Bromo-2-hydroxy-phenyl)-vinyl]-4-methoxy-phenyl}-1-hydroxymethyl-ethyl)-carbamic acid benzyl ester

Base Information

• Chemical Name: ((S)-2-{3-[1-(3-Bromo-2-hydroxy-phenyl)-vinyl]-4-methoxy-phenyl}-1-hydroxymethyl-ethyl)-carbamic acid benzyl ester
• CAS No.: 760979-97-3
• Molecular Formula: C₂₆H₂₆BrNO₅
• Molecular Weight: 512.4

Synonyms:((S)-2-{3-[1-(3-Bromo-2-hydroxy-phenyl)-vinyl]-4-methoxy-phenyl}-1-hydroxymethyl-ethyl)-carbamic acid benzyl ester

Chemical Property of ((S)-2-{3-[1-(3-Bromo-2-hydroxy-phenyl)-vinyl]-4-methoxy-phenyl}-1-hydroxymethyl-ethyl)-carbamic acid benzyl ester

Chemical Property:

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Technology Process of ((S)-2-{3-[1-(3-Bromo-2-hydroxy-phenyl)-vinyl]-4-methoxy-phenyl}-1-hydroxymethyl-ethyl)-carbamic acid benzyl ester

There total 1 articles about ((S)-2-{3-[1-(3-Bromo-2-hydroxy-phenyl)-vinyl]-4-methoxy-phenyl}-1-hydroxymethyl-ethyl)-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(S)-4-{3-[1-(3-Bromo-2-methoxymethoxy-phenyl)-vinyl]-4-methoxy-benzyl}-2,2-dimethyl-oxazolidine-3-carboxylic acid benzyl ester (761433-99-2) → ((S)-2-{3-[1-(3-Bromo-2-hydroxy-phenyl)-vinyl]-4-methoxy-phenyl}-1-hydroxymethyl-ethyl)-carbamic acid benzyl ester (760979-97-3)

Guidance literature:

With hydrogenchloride; In methanol; dichloromethane; at 25 ℃; for 12h;

DOI:10.1021/ja040090y

Reference yield: 95.0%

chloroacetonitrile (107-14-2) + ((S)-2-{3-[1-(3-Bromo-2-hydroxy-phenyl)-vinyl]-4-methoxy-phenyl}-1-hydroxymethyl-ethyl)-carbamic acid benzyl ester (760979-97-3) → ((S)-2-{3-[1-(3-Bromo-2-cyanomethoxy-phenyl)-vinyl]-4-methoxy-phenyl}-1-hydroxymethyl-ethyl)-carbamic acid benzyl ester (761434-00-8)

Guidance literature:

With potassium carbonate; In acetone; for 3h; Heating;

DOI:10.1021/ja040090y

Reference yield: 95.0%

bromoacetic acid methyl ester (96-32-2) + ((S)-2-{3-[1-(3-Bromo-2-hydroxy-phenyl)-vinyl]-4-methoxy-phenyl}-1-hydroxymethyl-ethyl)-carbamic acid benzyl ester (760979-97-3) → (2-{1-[5-((S)-2-Benzyloxycarbonylamino-3-hydroxy-propyl)-2-methoxy-phenyl]-vinyl}-6-bromo-phenoxy)-acetic acid methyl ester (760980-26-5)

Guidance literature:

With potassium carbonate; In acetone; for 3h; Heating;

DOI:10.1021/ja040091q

upstream raw materials:

(S)-4-{3-[1-(3-Bromo-2-methoxymethoxy-phenyl)-vinyl]-4-methoxy-benzyl}-2,2-dimethyl-oxazolidine-3-carboxylic acid benzyl ester

Downstream raw materials:

((S)-2-{3-[1-(3-Bromo-2-cyanomethoxy-phenyl)-vinyl]-4-methoxy-phenyl}-1-hydroxymethyl-ethyl)-carbamic acid benzyl ester

(2-{1-[5-((S)-2-Benzyloxycarbonylamino-3-hydroxy-propyl)-2-methoxy-phenyl]-vinyl}-6-bromo-phenoxy)-acetic acid methyl ester

(S)-4-{3-[1-(3-Bromo-2-cyanomethoxy-phenyl)-vinyl]-4-methoxy-benzyl}-2,2-dimethyl-oxazolidine-3-carboxylic acid benzyl ester

(S)-4-{3-[2-(3-Bromo-2-cyanomethoxy-phenyl)-oxiranyl]-4-methoxy-benzyl}-2,2-dimethyl-oxazolidine-3-carboxylic acid benzyl ester

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