μ-η2-(3-phenyl-2-propynal propylene glycol acetal)dicobalthexacarbonyl

Base Information

Chemical Name:μ-η2-(3-phenyl-2-propynal propylene glycol acetal)dicobalthexacarbonyl
CAS No.:1515868-45-7
Molecular Formula:C₁₈H₁₂Co₂O₈
Molecular Weight:474.275
Hs Code.:

Synonyms:μ-η2-(3-phenyl-2-propynal propylene glycol acetal)dicobalthexacarbonyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of μ-η2-(3-phenyl-2-propynal propylene glycol acetal)dicobalthexacarbonyl

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Technology Process of μ-η2-(3-phenyl-2-propynal propylene glycol acetal)dicobalthexacarbonyl

There total 2 articles about μ-η2-(3-phenyl-2-propynal propylene glycol acetal)dicobalthexacarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.7%

: 124069-76-7
hexacarbonyl μ-[η⁴-(1,1-diethoxy-3-phenyl-2-propyne)dicobalt]

: 504-63-2
trimethyleneglycol

: 1515868-45-7
μ-η2-(3-phenyl-2-propynal propylene glycol acetal)dicobalthexacarbonyl

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1021/om400718w

Reference yield:

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 1515868-45-7
μ-η2-(3-phenyl-2-propynal propylene glycol acetal)dicobalthexacarbonyl

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 3.5 h / 20 °C / Inert atmosphere; Schlenk technique

2: boron trifluoride diethyl etherate / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With boron trifluoride diethyl etherate; In diethyl ether; dichloromethane;
DOI:10.1021/om400718w

Reference yield: 21.9%

: 1515868-45-7
μ-η2-(3-phenyl-2-propynal propylene glycol acetal)dicobalthexacarbonyl

: 90108-98-8
μ-η2-(3-phenyl-2-propynal)dicobalthexacarbonyl

Guidance literature:: μ-η2-(3-phenyl-2-propynal propylene glycol acetal)dicobalthexacarbonyl; With trifluoromethylsulfonic anhydride; In dichloromethane; at -20 ℃; for 0.25h; Inert atmosphere; Schlenk technique;

With zinc; In dichloromethane; at -20 - 20 ℃; for 2.25h; Inert atmosphere; Schlenk technique;
DOI:10.1021/om400718w