tetraethyl 3-ethoxycarbonyl-N-<4-(methylamino)benzoyl>-3-aminopropylidene-1,1-bisphosphonate

Base Information

Chemical Name:tetraethyl 3-ethoxycarbonyl-N-<4-(methylamino)benzoyl>-3-aminopropylidene-1,1-bisphosphonate
CAS No.:120355-34-2
Molecular Formula:C₂₂H₃₈N₂O₉P₂
Molecular Weight:536.499
Hs Code.:

Synonyms:tetraethyl 3-ethoxycarbonyl-N-<4-(methylamino)benzoyl>-3-aminopropylidene-1,1-bisphosphonate

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Chemical Property of tetraethyl 3-ethoxycarbonyl-N-<4-(methylamino)benzoyl>-3-aminopropylidene-1,1-bisphosphonate

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Technology Process of tetraethyl 3-ethoxycarbonyl-N-<4-(methylamino)benzoyl>-3-aminopropylidene-1,1-bisphosphonate

There total 3 articles about tetraethyl 3-ethoxycarbonyl-N-<4-(methylamino)benzoyl>-3-aminopropylidene-1,1-bisphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120355-33-1
4,4-Bis-(diethoxy-phosphoryl)-2-{4-[methyl-(2,2,2-trichloro-ethoxycarbonyl)-amino]-benzoylamino}-butyric acid ethyl ester

: 120355-34-2
tetraethyl 3-ethoxycarbonyl-N-<4-(methylamino)benzoyl>-3-aminopropylidene-1,1-bisphosphonate

Guidance literature:: With potassium dihydrogenphosphate; zinc; In tetrahydrofuran; water; for 24h; Yield given; Ambient temperature;
DOI:10.1016/0223-5234(92)90117-J

Reference yield:

: 120355-30-8
2-amino-4,4-bis(diethylphosphono)butanoic acid ethyl ester

: 120355-34-2
tetraethyl 3-ethoxycarbonyl-N-<4-(methylamino)benzoyl>-3-aminopropylidene-1,1-bisphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / triethylamine / tetrahydrofuran / 1 h / Ambient temperature

2: KH₂PO₄, Zn / H₂O; tetrahydrofuran / 24 h / Ambient temperature

With potassium dihydrogenphosphate; triethylamine; zinc; In tetrahydrofuran; water;
DOI:10.1016/0223-5234(92)90117-J

Reference yield:

: (4-Chlorocarbonyl-phenyl)-methyl-carbamic acid 2,2,2-trichloro-ethyl ester

: 120355-34-2
tetraethyl 3-ethoxycarbonyl-N-<4-(methylamino)benzoyl>-3-aminopropylidene-1,1-bisphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / triethylamine / tetrahydrofuran / 1 h / Ambient temperature

2: KH₂PO₄, Zn / H₂O; tetrahydrofuran / 24 h / Ambient temperature

With potassium dihydrogenphosphate; triethylamine; zinc; In tetrahydrofuran; water;
DOI:10.1016/0223-5234(92)90117-J