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1H-Pyrrolo[3,2,1-de]phenanthridin-1-ol,2,4,5,- 7,11b,11c-hexahydro-9,10-dimethoxy-,(1R,- 11bS,11cS)-

Base Information
  • Chemical Name:1H-Pyrrolo[3,2,1-de]phenanthridin-1-ol,2,4,5,- 7,11b,11c-hexahydro-9,10-dimethoxy-,(1R,- 11bS,11cS)-
  • CAS No.:548-11-8
  • Molecular Formula:C17H21NO3
  • Molecular Weight:287.35
  • Hs Code.:
  • Mol file:548-11-8.mol
1H-Pyrrolo[3,2,1-de]phenanthridin-1-ol,2,4,5,- 7,11b,11c-hexahydro-9,10-dimethoxy-,(1R,- 11bS,11cS)-

Synonyms:Pluviin;pluviine;

Suppliers and Price of 1H-Pyrrolo[3,2,1-de]phenanthridin-1-ol,2,4,5,- 7,11b,11c-hexahydro-9,10-dimethoxy-,(1R,- 11bS,11cS)-
Supply Marketing:
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 4 raw suppliers
Chemical Property of 1H-Pyrrolo[3,2,1-de]phenanthridin-1-ol,2,4,5,- 7,11b,11c-hexahydro-9,10-dimethoxy-,(1R,- 11bS,11cS)-
Chemical Property:
  • Melting Point:225-7°C 
  • PSA:41.93000 
  • LogP:2.00420 
Purity/Quality:

99% *data from raw suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
  • Description First isolated from Lycoris radiata, this alkaloid has since been found in several species of Narcissus. It is strongly laevorotatory with [α]D - 170.5° (c 0.18, EtOH) or - 151 ° (c 0.42, CHCI3). The ultraviolet spectrum consists of a single absorption maximum at 282 mJI. The salts and derivatives crystallize readily and include the hydriodide, m.p. 237°C (dec.); the perchlorate, m.p. 260°C (dec.), the methiodide, m.p. 259-261°C (dec.); [α]29D~l - 129° (c 0.39, H20); the methoperchlorate, m.p. 239-241°C and the O-acetate, m.p. 184°C. Two methoxyl groups and a non-phenolic hydroxyl group are present.
Technology Process of 1H-Pyrrolo[3,2,1-de]phenanthridin-1-ol,2,4,5,- 7,11b,11c-hexahydro-9,10-dimethoxy-,(1R,- 11bS,11cS)-

There total 2 articles about 1H-Pyrrolo[3,2,1-de]phenanthridin-1-ol,2,4,5,- 7,11b,11c-hexahydro-9,10-dimethoxy-,(1R,- 11bS,11cS)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Guidance literature:
With palladium on activated charcoal; ethanol; acetic acid; Hydrogenation;
DOI:10.1021/ja01549a073
Guidance literature:
With methanol; diethyl ether;
DOI:10.1039/jr9590000172
Guidance literature:
at 100 ℃; Behandeln des Reaktionsgemisches mit wss.Salzsaeure;
upstream raw materials:

diazomethane

Downstream raw materials:

Vasconine

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