Agn-PC-0ngk3K

Base Information

Chemical Name:Agn-PC-0ngk3K
CAS No.:65367-77-3
Molecular Formula:C17H17NO2
Molecular Weight:267.3224
Hs Code.:
NSC Number:276735
DSSTox Substance ID:DTXSID70456737
ChEMBL ID:CHEMBL3248105

Synonyms:65367-77-3;AGN-PC-0NGK3K;CHEMBL3248105;DTXSID70456737;NSC276735;NSC-276735;O(C)c1cc2c(cc1OC)cn3CCc4cccc2c34;Pyrrolo[3,1-de]phenanthridinium, 4,5-dihydro-9,10-dimethoxy-, chloride

Suppliers and Price of Agn-PC-0ngk3K

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Agn-PC-0ngk3K

Chemical Property:

Vapor Pressure:9.52E-14mmHg at 25°C
Boiling Point:586.7°Cat760mmHg
Flash Point:257.1°C
Density:1.26g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:301.0869564
Heavy Atom Count:21
Complexity:361

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C2C3=CC=CC4=C3[N+](=CC2=C1)CC4)OC.[Cl-]

Technology Process of Agn-PC-0ngk3K

There total 8 articles about Agn-PC-0ngk3K which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 155206-75-0
tert-Butyl 7-(2-formyl-4,5-dimethoxyphenyl)-2,3-dihydroindole-1-carboxylate

: 65367-77-3
Vasconine

Guidance literature:: With hydrogenchloride; In chloroform; at 20 ℃; for 0.75h;
DOI:10.1002/adsc.200900499

Reference yield:

: 61203-53-0
2-iodo-4,5-dimethoxybenzaldehyde

: 65367-77-3
Vasconine

Guidance literature:: Multi-step reaction with 4 steps

2: 1.) sec-BuLi, N,N,N',N'-tetramethylethylenediamine, CuI-P(EtO)3 / 1.) ether, cyclohexane, -50 to -40 deg C, 2 h; -45 deg C, 30 min, 2.) r.t., 18 h

3: 1 M aq. HCl / tetrahydrofuran / 0.5 h / Heating

4: HCl / CHCl₃ / 0.25 h / Ambient temperature

With hydrogenchloride; triethylphosphite copper(I) iodide complex; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; chloroform;
DOI:10.1021/jo00091a049

Reference yield:

: 2-Iodo-4,5-dimethoxybenzaldehyde cyclohexylimine

: 65367-77-3
Vasconine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sec-BuLi, N,N,N',N'-tetramethylethylenediamine, CuI-P(EtO)3 / 1.) ether, cyclohexane, -50 to -40 deg C, 2 h; -45 deg C, 30 min, 2.) r.t., 18 h

2: 1 M aq. HCl / tetrahydrofuran / 0.5 h / Heating

3: HCl / CHCl₃ / 0.25 h / Ambient temperature

With hydrogenchloride; triethylphosphite copper(I) iodide complex; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; chloroform;
DOI:10.1021/jo00091a049