C₃₇H₄₄ClN₃O₁₃

Base Information

Chemical Name:C₃₇H₄₄ClN₃O₁₃
CAS No.:1312610-70-0
Molecular Formula:C₃₇H₄₄ClN₃O₁₃
Molecular Weight:774.222
Hs Code.:

C<sub>37</sub>H<sub>44</sub>ClN<sub>3</sub>O<sub>13</sub>

Synonyms:C₃₇H₄₄ClN₃O₁₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₇H₄₄ClN₃O₁₃

Chemical Property:

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Technology Process of C₃₇H₄₄ClN₃O₁₃

There total 8 articles about C₃₇H₄₄ClN₃O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 1312610-69-7
C₁₇H₁₂Br₂ClNO₅

: 1312610-70-0
C₃₇H₄₄ClN₃O₁₃

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 126463-85-2
4-acetylamino-5-chloro-2-methoxy-3-nitro-benzoic acid methyl ester

: 1312610-70-0
C₃₇H₄₄ClN₃O₁₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: sulfuric acid / methanol / 7 h / Reflux

2.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

4.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / Reflux

6.1: dichloromethane; diethyl ether / 2 h / -5 - 20 °C

6.2: -5 - 20 °C

7.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

With tert.-butylnitrite; oxalyl dichloride; lithium hydroxide monohydrate; sulfuric acid; water; sodium carbonate; N-ethyl-N,N-diisopropylamine; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; toluene; acetonitrile; 3.1: Suzuki Coupling;

Reference yield:

: 457947-61-4
4-amino-5-chloro-2-methoxy-3-nitro-benzoic acid methyl ester

: 1312610-70-0
C₃₇H₄₄ClN₃O₁₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

3.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / Reflux

5.1: dichloromethane; diethyl ether / 2 h / -5 - 20 °C

5.2: -5 - 20 °C

6.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

With tert.-butylnitrite; oxalyl dichloride; lithium hydroxide monohydrate; water; sodium carbonate; N-ethyl-N,N-diisopropylamine; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; toluene; acetonitrile; 2.1: Suzuki Coupling;