3,3-diethyl-5,5-dimethyl-1-(2’,6’-diisopropylphenyl)pyrrolidin-2-ylidene

Base Information

• Chemical Name: 3,3-diethyl-5,5-dimethyl-1-(2’,6’-diisopropylphenyl)pyrrolidin-2-ylidene
• CAS No.: 1508320-23-7
• Molecular Formula: C₂₂H₃₅N
• Molecular Weight: 313.527

Synonyms:3,3-diethyl-5,5-dimethyl-1-(2’,6’-diisopropylphenyl)pyrrolidin-2-ylidene

Chemical Property of 3,3-diethyl-5,5-dimethyl-1-(2’,6’-diisopropylphenyl)pyrrolidin-2-ylidene

Chemical Property:

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Technology Process of 3,3-diethyl-5,5-dimethyl-1-(2’,6’-diisopropylphenyl)pyrrolidin-2-ylidene

There total 2 articles about 3,3-diethyl-5,5-dimethyl-1-(2’,6’-diisopropylphenyl)pyrrolidin-2-ylidene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H36N(1+)*BF4(1-) → 3,3-diethyl-5,5-dimethyl-1-(2’,6’-diisopropylphenyl)pyrrolidin-2-ylidene (1508320-23-7)

Guidance literature:

With potassium hexamethylsilazane; In diethyl ether; Inert atmosphere;

DOI:10.1021/jacs.8b08545 DOI:10.1021/jacs.9b04249

Reference yield:

C22H33N + C22H35BrN(1+)*Br(1-) → 3,3-diethyl-5,5-dimethyl-1-(2’,6’-diisopropylphenyl)pyrrolidin-2-ylidene (1508320-23-7) + C22H33BrN(1+)*Br(1-)

Guidance literature:

In benzene-d6; for 0.5h; Inert atmosphere;

DOI:10.1021/jacs.7b04640

Reference yield: 90.0%

(tetrahydrothiophene)gold(I) chloride (39929-21-0) + 3,3-diethyl-5,5-dimethyl-1-(2’,6’-diisopropylphenyl)pyrrolidin-2-ylidene (1508320-23-7) + lithium trifluoromethanesulfonate (33454-82-9) → C44H70AuN2(1+)*CF3O3S(1-)

Guidance literature:

(tetrahydrothiophene)gold(I) chloride; 3,3-diethyl-5,5-dimethyl-1-(2’,6’-diisopropylphenyl)pyrrolidin-2-ylidene; In tetrahydrofuran; at -78 - 20 ℃; for 16h; Inert atmosphere;

lithium trifluoromethanesulfonate; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1002/chem.202004317

Downstream raw materials:

C₄₀H₆₂Cl₂N₂Si

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