methyl N-glycinate

Base Information

• Chemical Name: methyl N-glycinate
• CAS No.: 81478-01-5
• Molecular Formula: C₁₈H₁₈N₂O₃
• Molecular Weight: 310.353

Synonyms:methyl N-glycinate

Chemical Property of methyl N-glycinate

Chemical Property:

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Technology Process of methyl N-glycinate

There total 2 articles about methyl N-glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

Benzophenone imine (1013-88-3) + glycylglycine methyl ester hydrochloride (2776-60-5) → methyl N-glycinate (81478-01-5)

Guidance literature:

In dichloromethane; for 24h; Ambient temperature;

DOI:10.1021/jo00134a030

Reference yield: 29.0%

ethyl N-glycinate + methyl iodide (74-88-4) → methyl N-glycinate (81478-01-5)

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; Ambient temperature;

Reference yield: 90.0%

methyl N-glycinate (81478-01-5) + methyl iodide (74-88-4) → methyl N-glycinate

Guidance literature:

With potassium hydroxide; tetra-(n-butyl)ammonium iodide; In dimethyl sulfoxide; acetonitrile; at 15 - 20 ℃; for 2h;

upstream raw materials:

Benzophenone imine

glycylglycine methyl ester hydrochloride

methyl iodide

Downstream raw materials:

[PdCl((C₆H₄)(C₆H₅)CNCH₂CONHCH₂CO₂CH₃)]2

[PdCl(NC₅H₅)((C₆H₄)(C₆H₅)CNCH₂CONHCH₂CO₂CH₃)]

[PdCl(P(C₆H₅)3)((C₆H₄)(C₆H₅)CNCH₂CONHCH₂CO₂CH₃)]

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