N-(2,4,6-trimethylphenyl)-4-nitrobenzenesulfinamide

Base Information

Chemical Name:N-(2,4,6-trimethylphenyl)-4-nitrobenzenesulfinamide
CAS No.:32110-47-7
Molecular Formula:C₁₅H₁₆N₂O₃S
Molecular Weight:304.37
Hs Code.:

Synonyms:N-(2,4,6-trimethylphenyl)-4-nitrobenzenesulfinamide

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Chemical Property of N-(2,4,6-trimethylphenyl)-4-nitrobenzenesulfinamide

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Technology Process of N-(2,4,6-trimethylphenyl)-4-nitrobenzenesulfinamide

There total 4 articles about N-(2,4,6-trimethylphenyl)-4-nitrobenzenesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1365659-48-8
C₁₅H₁₆N₂O₂S

: 32110-47-7
N-(2,4,6-trimethylphenyl)-4-nitrobenzenesulfinamide

Guidance literature:: With potassium fluoride; 3-chloro-benzenecarboperoxoic acid; In water; acetonitrile; at 0 ℃; for 0.25h;
DOI:10.1080/00397911.2010.543748

Reference yield: 55.0%

: 26760-22-5
methyl p-nitrobenzenesulphinate

: 88-05-1
2,4,6-trimethylaniline

: 32110-47-7
N-(2,4,6-trimethylphenyl)-4-nitrobenzenesulfinamide

Guidance literature:: 2,4,6-trimethylaniline; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h; Inert atmosphere;

methyl p-nitrobenzenesulphinate; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.1c04122

Reference yield:

: 100-32-3
di(p-nitrophenyl) disulfide

: 32110-47-7
N-(2,4,6-trimethylphenyl)-4-nitrobenzenesulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide / dichloromethane / 0 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

With N-Bromosuccinimide; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/acs.orglett.1c04122