2,4-Dinitrobiphenyl

Base Information

Chemical Name:2,4-Dinitrobiphenyl
CAS No.:2486-04-6
Molecular Formula:C12H8N2O4
Molecular Weight:244.207
Hs Code.:2904209090
NSC Number:8739
DSSTox Substance ID:DTXSID10179559
Nikkaji Number:J1.880.133G
Mol file:2486-04-6.mol

Synonyms:2,4-Dinitrobiphenyl;2486-04-6;2,4-DINITRODIPHENYL;CCRIS 4053;NSC8739;NSC 8739;SCHEMBL2137404;DTXSID10179559;NSC-8739

Suppliers and Price of 2,4-Dinitrobiphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2,4-Dinitrobiphenyl

Chemical Property:

Vapor Pressure:1.07E-05mmHg at 25°C
Boiling Point:382°C at 760 mmHg
Flash Point:184.1°C
PSA：91.64000
Density:1.368g/cm³
LogP:4.21640
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:244.04840674
Heavy Atom Count:18
Complexity:317

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 2,4-Dinitrobiphenyl

There total 2 articles about 2,4-Dinitrobiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 709-49-9
1-iodo-2,4-dinitrobenzene

: 934-56-5
trimethyl(phenyl)stannane

: 92-52-4,1594-86-1
biphenyl

: 2486-04-6
2,4-dinitrobiphenyl

Guidance literature:: iodophenylbis(triphenylphosphine)palladium; In 1,2-dichloro-ethane; at 120 - 130 ℃; for 2h; Yields of byproduct given;

Reference yield: 40.0%

: 934-56-5
trimethyl(phenyl)stannane

: 78294-96-9
C₄₂H₃₃IN₂O₄P₂Pd

: 92-52-4,1594-86-1
biphenyl

: 2486-04-6
2,4-dinitrobiphenyl

Guidance literature:: In 1,2-dichloro-ethane; at 120 - 130 ℃; for 2h;

Reference yield:

: 2486-04-6
2,4-dinitrobiphenyl

: 188107-70-2
9-methyl-2-nitrocarbazole

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine / 1,2-dichloro-benzene / 6 h / Reflux

2: sodium hydroxide / N,N-dimethyl-formamide / 4 h / 2 °C

With triphenylphosphine; sodium hydroxide; In N,N-dimethyl-formamide; 1,2-dichloro-benzene;
DOI:10.1016/j.bmcl.2016.11.068